3-hydroxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

Base Information

Chemical Name:3-hydroxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether
CAS No.:1010094-05-9
Molecular Formula:C₂₂H₂₆O₁₀
Molecular Weight:450.442
Hs Code.:

Synonyms:3-hydroxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

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Chemical Property of 3-hydroxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

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Technology Process of 3-hydroxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

There total 5 articles about 3-hydroxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1010094-03-7
3-benzyloxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

: 1010094-05-9
3-hydroxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1016/j.tetlet.2007.11.154

Reference yield:

: 1010094-01-5
C₂₅H₂₈O₈

: 1010094-05-9
3-hydroxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 9 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 760.05 Torr

With pyridine; palladium 10% on activated carbon; hydrogen; In methanol;
DOI:10.1016/j.tet.2011.01.004

Reference yield:

: 1010093-99-8
dimethyl 3-benzyloxy-2,2',3',4'-tetramethoxy-1,1'-diphenylether-5,6'-dicarboxylate

: 1010094-05-9
3-hydroxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

2: pyridine / 9 h / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 760.05 Torr

With pyridine; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol;
DOI:10.1016/j.tet.2011.01.004