3-benzyloxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

Base Information

Chemical Name:3-benzyloxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether
CAS No.:1010094-03-7
Molecular Formula:C₂₉H₃₂O₁₀
Molecular Weight:540.567
Hs Code.:

Synonyms:3-benzyloxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

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Chemical Property of 3-benzyloxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

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Technology Process of 3-benzyloxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

There total 4 articles about 3-benzyloxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1010094-01-5
C₂₅H₂₈O₈

: 108-24-7
acetic anhydride

: 1010094-03-7
3-benzyloxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

Guidance literature:: With pyridine;
DOI:10.1016/j.tetlet.2007.11.154

Reference yield:

: 1010093-99-8
dimethyl 3-benzyloxy-2,2',3',4'-tetramethoxy-1,1'-diphenylether-5,6'-dicarboxylate

: 1010094-03-7
3-benzyloxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

2: pyridine / 9 h / 20 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1016/j.tet.2011.01.004

Reference yield:

: 135388-93-1
5-Benzyloxy-3-hydroxy-4-methoxybenzoesaeuremethylester

: 1010094-03-7
3-benzyloxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

Guidance literature:: Multi-step reaction with 3 steps

1: copper / 4 h / 200 °C / Inert atmosphere; neat (no solvent)

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3: pyridine / 9 h / 20 °C

With pyridine; lithium aluminium tetrahydride; copper; In tetrahydrofuran; 1: Ullmann condensation;
DOI:10.1016/j.tet.2011.01.004