5-(acetoxymethyl)-3-(6-(acetoxymethyl)-2,3,4-trimethoxyphenoxy)-2-methoxyphenyl 2-iodo-3,4,5-trimethoxybenzoate

Base Information

Chemical Name:5-(acetoxymethyl)-3-(6-(acetoxymethyl)-2,3,4-trimethoxyphenoxy)-2-methoxyphenyl 2-iodo-3,4,5-trimethoxybenzoate
CAS No.:1010094-07-1
Molecular Formula:C₃₂H₃₅IO₁₄
Molecular Weight:770.526
Hs Code.:

Synonyms:5-(acetoxymethyl)-3-(6-(acetoxymethyl)-2,3,4-trimethoxyphenoxy)-2-methoxyphenyl 2-iodo-3,4,5-trimethoxybenzoate

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Chemical Property of 5-(acetoxymethyl)-3-(6-(acetoxymethyl)-2,3,4-trimethoxyphenoxy)-2-methoxyphenyl 2-iodo-3,4,5-trimethoxybenzoate

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Technology Process of 5-(acetoxymethyl)-3-(6-(acetoxymethyl)-2,3,4-trimethoxyphenoxy)-2-methoxyphenyl 2-iodo-3,4,5-trimethoxybenzoate

There total 6 articles about 5-(acetoxymethyl)-3-(6-(acetoxymethyl)-2,3,4-trimethoxyphenoxy)-2-methoxyphenyl 2-iodo-3,4,5-trimethoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1010094-05-9
3-hydroxy-5,6'-bis(acetoxymethyl)-2,2',3',4'-tetramethoxy-1,1'-diphenylether

: 98799-41-8
2-iodo-3,4,5-trimethoxybenzoic acid

: 1010094-07-1
5-(acetoxymethyl)-3-(6-(acetoxymethyl)-2,3,4-trimethoxyphenoxy)-2-methoxyphenyl 2-iodo-3,4,5-trimethoxybenzoate

Guidance literature:: With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane;
DOI:10.1016/j.tetlet.2007.11.154

Reference yield:

: 1010094-01-5
C₂₅H₂₈O₈

: 1010094-07-1
5-(acetoxymethyl)-3-(6-(acetoxymethyl)-2,3,4-trimethoxyphenoxy)-2-methoxyphenyl 2-iodo-3,4,5-trimethoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 9 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 760.05 Torr

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 15 h / 20 °C

With pyridine; dmap; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane;
DOI:10.1016/j.tet.2011.01.004

Reference yield:

: 1010093-99-8
dimethyl 3-benzyloxy-2,2',3',4'-tetramethoxy-1,1'-diphenylether-5,6'-dicarboxylate

: 1010094-07-1
5-(acetoxymethyl)-3-(6-(acetoxymethyl)-2,3,4-trimethoxyphenoxy)-2-methoxyphenyl 2-iodo-3,4,5-trimethoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

2: pyridine / 9 h / 20 °C

3: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C / 760.05 Torr

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 15 h / 20 °C

With pyridine; dmap; lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tet.2011.01.004