N-{2-[7-benzyl-5-(4-benzyloxyphenyl)-1-methyl-4,8-dioxo-1,4,7,8-tetrahydropyrrolo[3,2-f]indol-3-yl]ethyl}-N-methylcarbamic acid tert-butyl ester

Base Information

Chemical Name:N-{2-[7-benzyl-5-(4-benzyloxyphenyl)-1-methyl-4,8-dioxo-1,4,7,8-tetrahydropyrrolo[3,2-f]indol-3-yl]ethyl}-N-methylcarbamic acid tert-butyl ester
CAS No.:1430737-16-8
Molecular Formula:C₃₉H₃₉N₃O₅
Molecular Weight:629.756
Hs Code.:

Synonyms:N-{2-[7-benzyl-5-(4-benzyloxyphenyl)-1-methyl-4,8-dioxo-1,4,7,8-tetrahydropyrrolo[3,2-f]indol-3-yl]ethyl}-N-methylcarbamic acid tert-butyl ester

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Chemical Property of N-{2-[7-benzyl-5-(4-benzyloxyphenyl)-1-methyl-4,8-dioxo-1,4,7,8-tetrahydropyrrolo[3,2-f]indol-3-yl]ethyl}-N-methylcarbamic acid tert-butyl ester

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Technology Process of N-{2-[7-benzyl-5-(4-benzyloxyphenyl)-1-methyl-4,8-dioxo-1,4,7,8-tetrahydropyrrolo[3,2-f]indol-3-yl]ethyl}-N-methylcarbamic acid tert-butyl ester

There total 1 articles about N-{2-[7-benzyl-5-(4-benzyloxyphenyl)-1-methyl-4,8-dioxo-1,4,7,8-tetrahydropyrrolo[3,2-f]indol-3-yl]ethyl}-N-methylcarbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1430737-14-6
2-[7-benzyl-5-(4-benzyloxyphenyl)-4,8-dioxo-1-tosyl-1,4,7,8-tetrahydro-pyrrolo[3,2-f]indol-3-yl]ethylcarbamic acid tert-butyl ester

: 74-88-4
methyl iodide

: 1430737-15-7
N-{2-[7-benzyl-5-(4-benzyloxyphenyl)-4,8-dioxo-1-tosyl-1,4,7,8-tetrahydropyrrolo[3,2-f]indol-3-yl]ethyl}-N-methylcarbamic acid tert-butyl ester

: 1430737-16-8
N-{2-[7-benzyl-5-(4-benzyloxyphenyl)-1-methyl-4,8-dioxo-1,4,7,8-tetrahydropyrrolo[3,2-f]indol-3-yl]ethyl}-N-methylcarbamic acid tert-butyl ester

Guidance literature:: 2-[7-benzyl-5-(4-benzyloxyphenyl)-4,8-dioxo-1-tosyl-1,4,7,8-tetrahydro-pyrrolo[3,2-f]indol-3-yl]ethylcarbamic acid tert-butyl ester; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 25 ℃; for 30h;
DOI:10.1016/j.tet.2013.03.052

Reference yield: 55.0%

: 1430737-16-8
N-{2-[7-benzyl-5-(4-benzyloxyphenyl)-1-methyl-4,8-dioxo-1,4,7,8-tetrahydropyrrolo[3,2-f]indol-3-yl]ethyl}-N-methylcarbamic acid tert-butyl ester

: 1430737-18-0
N-{2-[5-(4-hydroxyphenyl)-1-methyl-4,8-dioxo-1,4,7,8-tetrahydropyrrolo[3,2-f]-indol-3-yl]ethyl}-N-methylcarbamic acid tert-butyl ester

Guidance literature:: With ammonium formate; palladium; In ethanol; for 15h; Reflux;
DOI:10.1016/j.tet.2013.03.052

Reference yield:

: 1430737-16-8
N-{2-[7-benzyl-5-(4-benzyloxyphenyl)-1-methyl-4,8-dioxo-1,4,7,8-tetrahydropyrrolo[3,2-f]indol-3-yl]ethyl}-N-methylcarbamic acid tert-butyl ester

: C₃₅H₃₁N₃O₅

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 25 ℃; for 2h; Reagent/catalyst; Temperature;
DOI:10.1016/j.tet.2013.03.052