N-[2-methyl-5-(2-morpholinopyrid-4-ylcarbonylamino)phenyl]-5-chloro-2-nitrobenzamide

Base Information

• Chemical Name: N-[2-methyl-5-(2-morpholinopyrid-4-ylcarbonylamino)phenyl]-5-chloro-2-nitrobenzamide
• CAS No.: 263270-28-6
• Molecular Formula: C₂₄H₂₂ClN₅O₅
• Molecular Weight: 495.922

Synonyms:N-[2-methyl-5-(2-morpholinopyrid-4-ylcarbonylamino)phenyl]-5-chloro-2-nitrobenzamide

Chemical Property of N-[2-methyl-5-(2-morpholinopyrid-4-ylcarbonylamino)phenyl]-5-chloro-2-nitrobenzamide

Chemical Property:

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Technology Process of N-[2-methyl-5-(2-morpholinopyrid-4-ylcarbonylamino)phenyl]-5-chloro-2-nitrobenzamide

There total 2 articles about N-[2-methyl-5-(2-morpholinopyrid-4-ylcarbonylamino)phenyl]-5-chloro-2-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxalyl dichloride (79-37-8) + 5-chloro-2-nitrobenzoic acid (2516-95-2) + N-(3-amino-4-methylphenyl)-2-morpholinopyridine-4-carboxamide (258503-86-5) → N-[2-methyl-5-(2-morpholinopyrid-4-ylcarbonylamino)phenyl]-5-chloro-2-nitrobenzamide (263270-28-6)

Guidance literature:

With triethylamine; In dichloromethane hydrate; diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

2-chloropyridine-4-carbonyl chloride (65287-34-5) + 4-Methyl-3-nitroanilin (119-32-4) → N-[2-methyl-5-(2-morpholinopyrid-4-ylcarbonylamino)phenyl]-5-chloro-2-nitrobenzamide (263270-28-6) + 2-chloro-N-(4-methyl-3-nitrophenyl) pyridine-4-carboxamide (258503-84-3)

Guidance literature:

With triethylamine; In dichloromethane;

Reference yield:

N-[2-methyl-5-(2-morpholinopyrid-4-ylcarbonylamino)phenyl]-5-chloro-2-nitrobenzamide (263270-28-6) + N,N,N'-trimethylpropane-1,3-diamine (4543-96-8) → N-[2-methyl-5-(2-morpholinopyrid-4-ylcarbonylamino)phenyl]-5-[N-(3-dimethylaminopropyl)-N-methylamino]-2-nitrobenzamide (263268-88-8)

Guidance literature:

In diethyl ether; water;

upstream raw materials:

oxalyl dichloride

5-chloro-2-nitrobenzoic acid

N-(3-amino-4-methylphenyl)-2-morpholinopyridine-4-carboxamide

2-chloropyridine-4-carbonyl chloride

Downstream raw materials:

N-[2-methyl-5-(2-morpholinopyrid-4-ylcarbonylamino)phenyl]-5-[N-(3-dimethylaminopropyl)-N-methylamino]-2-nitrobenzamide

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