C₃₂H₃₃NO₇

Base Information

Chemical Name:C₃₂H₃₃NO₇
CAS No.:1265173-13-4
Molecular Formula:C₃₂H₃₃NO₇
Molecular Weight:543.617
Hs Code.:

C<sub>32</sub>H<sub>33</sub>NO<sub>7</sub>

Synonyms:C₃₂H₃₃NO₇

Suppliers and Price of C₃₂H₃₃NO₇

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₂H₃₃NO₇

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₂H₃₃NO₇

There total 24 articles about C₃₂H₃₃NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₂₇NO₇

: 100-39-0
benzyl bromide

: 1265173-13-4
C₃₂H₃₃NO₇

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1002/asia.201000602

Reference yield:

: 1265173-20-3
C₂₂H₂₈O₇S

: 1265173-13-4
C₃₂H₃₃NO₇

Guidance literature:: Multi-step reaction with 16 steps

1.1: acetic anhydride; dimethyl sulfoxide / 2 h / 50 °C

2.1: toluene / 4 h / -40 °C

3.1: magnesium / methanol / 2 h / 20 °C

4.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / 4 h / 20 °C

5.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 0.17 h / 0 °C

5.2: 0 - 20 °C

6.1: pyridine / dichloromethane / 2 h / 0 °C

7.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C

8.1: dichloromethane / 1 h / 0 °C

9.1: sodium carbonate / tert-butylbenzene / 24 h / 170 °C

10.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C

11.1: potassium carbonate / tetrahydrofuran; water / 3 h / 0 °C

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C

13.1: scandium tris(trifluoromethanesulfonate) / dichloromethane; water / 20 - 40 °C

14.1: Jones reagent / water; acetone / 0 - 20 °C

15.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 12 h / 20 °C

16.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

With pyridine; sodium chlorite; sodium dihydrogenphosphate; Jones reagent; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; acetic anhydride; sodium hydride; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; magnesium; dimethyl sulfoxide; triethylamine; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; tert-butylbenzene; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; mineral oil; tert-butyl alcohol; 4.1: Swern oxidation / 5.2: Horner-Wadsworth-Emmons olefination / 9.1: Overman rearrangement / 15.1: Kraus-Pinnick reaction;
DOI:10.1002/asia.201000602

Reference yield:

: 1265173-03-2
C₂₂H₂₆O₇S

: 1265173-13-4
C₃₂H₃₃NO₇

Guidance literature:: Multi-step reaction with 15 steps

1.1: toluene / 4 h / -40 °C

2.1: magnesium / methanol / 2 h / 20 °C

3.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / 4 h / 20 °C

4.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 0.17 h / 0 °C

4.2: 0 - 20 °C

5.1: pyridine / dichloromethane / 2 h / 0 °C

6.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C

7.1: dichloromethane / 1 h / 0 °C

8.1: sodium carbonate / tert-butylbenzene / 24 h / 170 °C

9.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C

10.1: potassium carbonate / tetrahydrofuran; water / 3 h / 0 °C

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C

12.1: scandium tris(trifluoromethanesulfonate) / dichloromethane; water / 20 - 40 °C

13.1: Jones reagent / water; acetone / 0 - 20 °C

14.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 12 h / 20 °C

15.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

With pyridine; sodium chlorite; sodium dihydrogenphosphate; Jones reagent; 2-methyl-but-2-ene; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; sodium hydride; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; magnesium; dimethyl sulfoxide; triethylamine; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; tert-butylbenzene; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; mineral oil; tert-butyl alcohol; 3.1: Swern oxidation / 4.2: Horner-Wadsworth-Emmons olefination / 8.1: Overman rearrangement / 14.1: Kraus-Pinnick reaction;
DOI:10.1002/asia.201000602