(((2-(2-iodophenyl)propan-2-yl)oxy)(trifluoromethyl)sulfane)

Base Information

• Chemical Name: (((2-(2-iodophenyl)propan-2-yl)oxy)(trifluoromethyl)sulfane)
• CAS No.: 1584705-82-7
• Molecular Formula: C₁₀H₁₀F₃IOS
• Molecular Weight: 362.155
• Mol file: 1584705-82-7.mol

Synonyms:(((2-(2-iodophenyl)propan-2-yl)oxy)(trifluoromethyl)sulfane)

Chemical Property of (((2-(2-iodophenyl)propan-2-yl)oxy)(trifluoromethyl)sulfane)

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (((2-(2-iodophenyl)propan-2-yl)oxy)(trifluoromethyl)sulfane)

There total 4 articles about (((2-(2-iodophenyl)propan-2-yl)oxy)(trifluoromethyl)sulfane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-(2-iodophenyl)propan-2-ol (69352-05-2) + 2-((trifluoromethyl)thio)benzo[d]isothiazol-3(2H)-one 1,1-dioxide → (((2-(2-iodophenyl)propan-2-yl)oxy)(trifluoromethyl)sulfane) (1584705-82-7)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 0.0833333h;

DOI:10.1002/anie.201403983

Reference yield: 92.0%

2-(2-iodophenyl)propan-2-ol (69352-05-2) + N-trifluoromethylthio-saccharin → (((2-(2-iodophenyl)propan-2-yl)oxy)(trifluoromethyl)sulfane) (1584705-82-7)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 0.0833333h;

DOI:10.1002/anie.201805859

Reference yield: 43.0%

1-chloro-1,3-dihydro-3,3-dimethyl-1,2-benziodoxole (69352-04-1) + silver(I) trifluoromethanethiolate (811-68-7) → (((2-(2-iodophenyl)propan-2-yl)oxy)(trifluoromethyl)sulfane) (1584705-82-7)

Guidance literature:

at 50 ℃; for 1h; Schlenk technique; Inert atmosphere; Sealed tube;

DOI:10.1016/j.jfluchem.2014.09.011

upstream raw materials:

2-(2-iodophenyl)propan-2-ol

1-chloro-1,3-dihydro-3,3-dimethyl-1,2-benziodoxole

silver(I) trifluoromethanethiolate

o-iodo-methyl-benzoic acid

Downstream raw materials:

[1,1′-biphenyl]-4-yl(trifluoromethyl)sulfane

(6-bromo-1-phenylhexan-2-yl)(trifluoromethyl)sulfane

(1-phenylpent-4-en-2-yl)(trifluoromethyl)sulfane

(1-(4-methoxyphenyl)hex-4-yn-2-yl)(trifluoromethyl)sulfane