6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-α/β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

Base Information

Chemical Name:6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-α/β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside
CAS No.:898528-03-5
Molecular Formula:C₆₉H₈₆Cl₃NO₁₃Si
Molecular Weight:1271.89
Hs Code.:

6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-α/β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

Synonyms:6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-α/β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

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Chemical Property of 6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-α/β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

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Technology Process of 6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-α/β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

There total 7 articles about 6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-α/β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 898528-02-4
6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-β-D-galactopyranoside

: 397249-84-2
phenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-1-thio-β-D-galactopyranoside

: 898528-03-5
6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-α/β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; MSAW-300; In various solvent(s); at -60 ℃; for 1h;
DOI:10.1248/cpb.54.485

Reference yield:

: 100-39-0
benzyl bromide

: 898528-03-5
6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-α/β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / NaH / dimethylformamide / 2 h / 0 °C

2: 81.2 percent / N-iodosuccinimide; trifluoromethanesulfonic acid; MSAW-300 / various solvent(s) / 1 h / -60 °C

3: 100 percent / p-toluenesulfonic acid / CHCl₃; methanol / 1 h / 20 °C

4: 70 percent / N-iodosuccinimide; trifluoromethanesulfonic acid; MSAW-300 / various solvent(s) / 1 h / -60 °C

With N-iodo-succinimide; trifluorormethanesulfonic acid; MSAW-300; sodium hydride; toluene-4-sulfonic acid; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1248/cpb.54.485

Reference yield:

: 225241-29-2
phenyl 6-O-(tert-butyldimethylsilyloxy)-1-thio-β-D-galactopyranoside

: 898528-03-5
6-N-(2,2,2-trichloroethoxycarbonyl)aminohexyl 2,3,4-tri-O-benzyl-6-O-tert-butyldimethylsilyl-α/β-D-galactopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / NaH / dimethylformamide / 2 h / 0 °C

2: 81.2 percent / N-iodosuccinimide; trifluoromethanesulfonic acid; MSAW-300 / various solvent(s) / 1 h / -60 °C

3: 100 percent / p-toluenesulfonic acid / CHCl₃; methanol / 1 h / 20 °C

4: 70 percent / N-iodosuccinimide; trifluoromethanesulfonic acid; MSAW-300 / various solvent(s) / 1 h / -60 °C

With N-iodo-succinimide; trifluorormethanesulfonic acid; MSAW-300; sodium hydride; toluene-4-sulfonic acid; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1248/cpb.54.485