3-(4-Hydroxy-phenyl)-2-[(E)-tetrahydro-pyran-2-yloxyimino]-propionic acid

Base Information

Chemical Name:3-(4-Hydroxy-phenyl)-2-[(E)-tetrahydro-pyran-2-yloxyimino]-propionic acid
CAS No.:664994-80-3
Molecular Formula:C₁₄H₁₇NO₅
Molecular Weight:279.293
Hs Code.:

Synonyms:3-(4-Hydroxy-phenyl)-2-[(E)-tetrahydro-pyran-2-yloxyimino]-propionic acid

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Chemical Property of 3-(4-Hydroxy-phenyl)-2-[(E)-tetrahydro-pyran-2-yloxyimino]-propionic acid

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Technology Process of 3-(4-Hydroxy-phenyl)-2-[(E)-tetrahydro-pyran-2-yloxyimino]-propionic acid

There total 2 articles about 3-(4-Hydroxy-phenyl)-2-[(E)-tetrahydro-pyran-2-yloxyimino]-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 6723-30-4
O-2-tetrahydro-2H-pyranhydroxylamine

: 156-39-8
4-hydroxyphenylpiruvic acid

: 664994-80-3
3-(4-Hydroxy-phenyl)-2-[(E)-tetrahydro-pyran-2-yloxyimino]-propionic acid

Guidance literature:: In ethanol; Heating;

Reference yield:

: 156-39-8
4-hydroxyphenylpiruvic acid

: 120104-92-9
O-(tetrahydro-2H-pyran-2-yl) hydroxylamine hydrochloride

: 664994-80-3
3-(4-Hydroxy-phenyl)-2-[(E)-tetrahydro-pyran-2-yloxyimino]-propionic acid

Guidance literature:: With sodium acetate; In ethanol; at 20 ℃; for 6h;
DOI:10.1016/j.tet.2005.05.038

Reference yield: 89.0%

: 664994-80-3
3-(4-Hydroxy-phenyl)-2-[(E)-tetrahydro-pyran-2-yloxyimino]-propionic acid

: 958255-23-7
{3-[4-(2-amino-ethyl)-2,6-dibromo-phenoxy]-propyl}-methyl-carbamic acid methyl ester

: [3-(2,6-dibromo-4-{2-[3-(4-hydroxy-phenyl)-2-(tetrahydro-pyran-2-yloxyimino)-propionylamino]-ethyl}-phenoxy)-propyl]-methyl-carbamic acid methyl ester

Guidance literature:: 3-(4-Hydroxy-phenyl)-2-[(E)-tetrahydro-pyran-2-yloxyimino]-propionic acid; With benzotriazol-1-ol; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

{3-[4-(2-amino-ethyl)-2,6-dibromo-phenoxy]-propyl}-methyl-carbamic acid methyl ester; In N,N-dimethyl-formamide; at 20 ℃; for 1h;