N-hydroxy-N-2-[(N-p-chlorophenyl)-3-pyrazolyloxymethyl]phenyl hydroxylamine

Base Information

Chemical Name:N-hydroxy-N-2-[(N-p-chlorophenyl)-3-pyrazolyloxymethyl]phenyl hydroxylamine
CAS No.:220898-42-0
Molecular Formula:C₁₆H₁₄ClN₃O₂
Molecular Weight:315.759
Hs Code.:

Synonyms:N-hydroxy-N-2-[(N-p-chlorophenyl)-3-pyrazolyloxymethyl]phenyl hydroxylamine

Suppliers and Price of N-hydroxy-N-2-[(N-p-chlorophenyl)-3-pyrazolyloxymethyl]phenyl hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
N-(2-(((1-(4-Chlorophenyl)-1H-pyrazol-3-yl)oxy)methyl)phenyl)hydroxylamine 97%
1g
$ 771.00

Total 3 raw suppliers

Chemical Property of N-hydroxy-N-2-[(N-p-chlorophenyl)-3-pyrazolyloxymethyl]phenyl hydroxylamine

Chemical Property:

Boiling Point:502.8±60.0 °C(Predicted)
Density:1.32±0.1 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

N-(2-(((1-(4-Chlorophenyl)-1H-pyrazol-3-yl)oxy)methyl)phenyl)hydroxylamine 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses N-(2-(((1-(4-Chlorophenyl)-1H-pyrazol-3-yl)oxy)methyl)phenyl)hydroxylamine is an intermediate for the synthesis of Pyraclostrobin-d6 (P840402). Isotope labelled Pyraclostrobin is a fungicide for use in seed grass and food crops.

Technology Process of N-hydroxy-N-2-[(N-p-chlorophenyl)-3-pyrazolyloxymethyl]phenyl hydroxylamine

There total 6 articles about N-hydroxy-N-2-[(N-p-chlorophenyl)-3-pyrazolyloxymethyl]phenyl hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.4%

: 220368-29-6
2-[(N-4-chlorophenyl)-1H-pyrazol-3-yloxymethyl]-1-nitrobenzene

: 220898-42-0
N-hydroxy-N-2-[(N-p-chlorophenyl)-3-pyrazolyloxymethyl]phenyl hydroxylamine

Guidance literature:: With platinum on activated charcoal; hydrogen; triphenylphosphine; In dimethyl sulfoxide; isopropyl alcohol; at 30 - 35 ℃; for 16h; under 825.083 Torr; Solvent; Reagent/catalyst; Temperature; Pressure; Autoclave;

Reference yield:

: 76205-19-1
1-(para-chlorophenyl)-3-hydroxypyrazole

: 220898-42-0
N-hydroxy-N-2-[(N-p-chlorophenyl)-3-pyrazolyloxymethyl]phenyl hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide; tetrabutylammomium bromide / methanol / 2 h / 50 °C / Large scale

2: hydrazine hydrate / 1,2-dichloro-ethane; ethanol / 3 h / 0 - 5 °C / 375.04 Torr / Inert atmosphere; Large scale

With hydrazine hydrate; tetrabutylammomium bromide; potassium hydroxide; In methanol; ethanol; 1,2-dichloro-ethane;

Reference yield:

: 3958-60-9
2-nitrophenylmethyl bromide

: 220898-42-0
N-hydroxy-N-2-[(N-p-chlorophenyl)-3-pyrazolyloxymethyl]phenyl hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide; tetrabutylammomium bromide / methanol / 2 h / 50 °C / Large scale

2: hydrazine hydrate / 1,2-dichloro-ethane; ethanol / 3 h / 0 - 5 °C / 375.04 Torr / Inert atmosphere; Large scale

With hydrazine hydrate; tetrabutylammomium bromide; potassium hydroxide; In methanol; ethanol; 1,2-dichloro-ethane;