(+)-phenylmethyl ((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

Base Information

Chemical Name:(+)-phenylmethyl ((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate
CAS No.:174626-07-4
Molecular Formula:C₃₁H₂₉NO₃
Molecular Weight:463.576
Hs Code.:

Synonyms:(+)-phenylmethyl ((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

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Chemical Property of (+)-phenylmethyl ((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

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Technology Process of (+)-phenylmethyl ((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

There total 3 articles about (+)-phenylmethyl ((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1315128-16-5
phenylmethyl formyl((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

: 174626-07-4
(+)-phenylmethyl ((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 1h;
DOI:10.1002/chem.201100649

Reference yield:

: cinnamyl methyl carbonate

: 174626-07-4
(+)-phenylmethyl ((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₃₂NO₃P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: potassium hydroxide / methanol / 1 h / 20 °C

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₃₂NO₃P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1002/chem.201100649

Reference yield:

: 69261-49-0
benzyl formylcarbamate

: 174626-07-4
(+)-phenylmethyl ((1R)-1-{[(triphenylmethyl)oxy]methyl}prop-2-en-1-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₃₂NO₃P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: potassium hydroxide / methanol / 1 h / 20 °C

With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C₃₇H₃₂NO₃P; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1002/chem.201100649