4-[2-Benzyloxy-5-((S)-2-benzyloxycarbonylamino-2-methoxycarbonyl-ethyl)-phenoxy]-benzoic acid tert-butyl ester

Base Information

Chemical Name:4-[2-Benzyloxy-5-((S)-2-benzyloxycarbonylamino-2-methoxycarbonyl-ethyl)-phenoxy]-benzoic acid tert-butyl ester
CAS No.:120363-14-6
Molecular Formula:C₃₆H₃₇NO₈
Molecular Weight:611.692
Hs Code.:

Synonyms:4-[2-Benzyloxy-5-((S)-2-benzyloxycarbonylamino-2-methoxycarbonyl-ethyl)-phenoxy]-benzoic acid tert-butyl ester

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Chemical Property of 4-[2-Benzyloxy-5-((S)-2-benzyloxycarbonylamino-2-methoxycarbonyl-ethyl)-phenoxy]-benzoic acid tert-butyl ester

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Technology Process of 4-[2-Benzyloxy-5-((S)-2-benzyloxycarbonylamino-2-methoxycarbonyl-ethyl)-phenoxy]-benzoic acid tert-butyl ester

There total 2 articles about 4-[2-Benzyloxy-5-((S)-2-benzyloxycarbonylamino-2-methoxycarbonyl-ethyl)-phenoxy]-benzoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120363-13-5
tert-butyl 4-iodobenzoate

: 105229-41-2
2-Benzyloxycarbonylamino-3-(4-benzyloxy-3-hydroxy-phenyl)-propionic acid methyl ester

: 120363-11-3,120363-14-6
N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-<(1,1-dimethylethoxy)carbonyl>phenoxy>-D-tyrosine methyl ester

: 120363-14-6
N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-<(1,1-dimethylethoxy)carbonyl>phenoxy>-L-tyrosine methyl ester

Guidance literature:: With copper(I) bromide dimethylsulfide complex; sodium hydride; In nitrobenzene; at 130 ℃; for 8h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(01)93709-8

Reference yield:

: 120363-13-5
tert-butyl 4-iodobenzoate

: 105229-41-2
2-Benzyloxycarbonylamino-3-(4-benzyloxy-3-hydroxy-phenyl)-propionic acid methyl ester

: 120363-11-3,120363-14-6
N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-<(1,1-dimethylethoxy)carbonyl>phenoxy>-D-tyrosine methyl ester

: 120363-14-6
N-<(Phenylmethoxy)carbonyl>-O-(phenylmethyl)-3-<4-<(1,1-dimethylethoxy)carbonyl>phenoxy>-L-tyrosine methyl ester

Guidance literature:: With copper(I) bromide dimethylsulfide complex; sodium hydride; In nitrobenzene; at 130 ℃; for 8h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(01)93709-8