4-bis(2'-tert-butyldimethylsilyloxyethyl)amino-N-tert-butyloxycarbonylaniline

Base Information

Chemical Name:4-bis(2'-tert-butyldimethylsilyloxyethyl)amino-N-tert-butyloxycarbonylaniline
CAS No.:244247-70-9
Molecular Formula:C₂₇H₅₂N₂O₄Si₂
Molecular Weight:524.892
Hs Code.:

Synonyms:4-bis(2'-tert-butyldimethylsilyloxyethyl)amino-N-tert-butyloxycarbonylaniline

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Chemical Property of 4-bis(2'-tert-butyldimethylsilyloxyethyl)amino-N-tert-butyloxycarbonylaniline

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Technology Process of 4-bis(2'-tert-butyldimethylsilyloxyethyl)amino-N-tert-butyloxycarbonylaniline

There total 3 articles about 4-bis(2'-tert-butyldimethylsilyloxyethyl)amino-N-tert-butyloxycarbonylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18226-17-0
N,N-bis(2-hydroxyethyl)-4-nitroaniline

: 244247-70-9
4-bis(2'-tert-butyldimethylsilyloxyethyl)amino-N-tert-butyloxycarbonylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / imidazole / dimethylformamide / 20 h / 20 °C

2: 95 percent / H₂ / Pd/C / tetrahydrofuran / 6 h

3: 100 percent / tetrahydrofuran / 16 h / 20 °C

With 1H-imidazole; hydrogen; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm020462i

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 244247-70-9
4-bis(2'-tert-butyldimethylsilyloxyethyl)amino-N-tert-butyloxycarbonylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / imidazole / dimethylformamide / 20 h / 20 °C

2: 95 percent / H₂ / Pd/C / tetrahydrofuran / 6 h

3: 100 percent / tetrahydrofuran / 16 h / 20 °C

With 1H-imidazole; hydrogen; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm020462i

Reference yield:

: 304015-61-0
N,N-bis(2-{[tert-butyldimethylsilyl]oxy}ethyl)-4-nitroaniline

: 244247-70-9
4-bis(2'-tert-butyldimethylsilyloxyethyl)amino-N-tert-butyloxycarbonylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / H₂ / Pd/C / tetrahydrofuran / 6 h

2: 100 percent / tetrahydrofuran / 16 h / 20 °C

With hydrogen; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/jm020462i