(3S,6R)-3-Allyl-6-isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one

Base Information

Chemical Name:(3S,6R)-3-Allyl-6-isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one
CAS No.:191284-36-3
Molecular Formula:C₁₇H₂₁NO₂
Molecular Weight:271.359
Hs Code.:

Synonyms:(3S,6R)-3-Allyl-6-isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one

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Chemical Property of (3S,6R)-3-Allyl-6-isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one

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Technology Process of (3S,6R)-3-Allyl-6-isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one

There total 3 articles about (3S,6R)-3-Allyl-6-isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1469-70-1
allyl ethyl carbonate

: (6R)-6-Isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one

: 191284-36-3
(3S,6R)-3-Allyl-6-isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one

Guidance literature:: palladium diacetate; triphenylphosphine; In tetrahydrofuran; for 12h; Ambient temperature;
DOI:10.1055/s-1999-3456

Reference yield: 62.0%

: 556-56-9
allyl iodid

: (6R)-6-Isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one

: 191284-36-3
(3S,6R)-3-Allyl-6-isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one

: (3R,6R)-3-Allyl-6-isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one

Guidance literature:: With tetrabutylammomium bromide; potassium carbonate; In acetonitrile; for 24h; Yields of byproduct given; Ambient temperature;
DOI:10.1055/s-1999-3456

Reference yield: 38.0%

: 107-05-1
3-chloroprop-1-ene

: (6R)-6-Isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one

: 191284-36-3
(3S,6R)-3-Allyl-6-isopropyl-3-methyl-5-phenyl-3,6-dihydro-2H-1,4-oxazin-2-one

Guidance literature:: With 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine; In various solvent(s); for 1h; Ambient temperature;
DOI:10.1055/s-1999-3456