1-mesityl-3-(pyridin-2-yl)-1H-imidazol-3-ium bromide

Base Information

Chemical Name:1-mesityl-3-(pyridin-2-yl)-1H-imidazol-3-ium bromide
CAS No.:455885-01-5
Molecular Formula:Br*C₁₇H₁₈N₃
Molecular Weight:344.254
Hs Code.:

Synonyms:1-mesityl-3-(pyridin-2-yl)-1H-imidazol-3-ium bromide

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Chemical Property of 1-mesityl-3-(pyridin-2-yl)-1H-imidazol-3-ium bromide

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Technology Process of 1-mesityl-3-(pyridin-2-yl)-1H-imidazol-3-ium bromide

There total 1 articles about 1-mesityl-3-(pyridin-2-yl)-1H-imidazol-3-ium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 109-04-6
2-bromo-pyridine

: 25364-44-7
N-(2,4,6-trimethylphenyl)imidazole

: 455885-01-5
1-mesityl-3-(pyridin-2-yl)-1H-imidazol-3-ium bromide

Guidance literature:: at 160 ℃; for 10h; Sealed tube;
DOI:10.1021/om500178e

Reference yield: 95.0%

: 12145-47-0
cis-dibromo-(cyclooctadiene)palladium(II)

: 455885-01-5
1-mesityl-3-(pyridin-2-yl)-1H-imidazol-3-ium bromide

: [PdBr₂(N-mesityl-N'-2-pyridylimidazolium)]

Guidance literature:: In dichloromethane; a soln. of imidazolium-compound in CH2Cl2 was aded dropwise to a soln. of Pd-complex in CH2Cl2, stirred at room temp. for 15 h with exclusion from light; filtered through Celite, volatiles were removed under reduced pressure, the solid was washed with diethyl ether, dried under vac., recrystd. from DMSO/diethyl ether; elem. anal.;
DOI:10.1021/om201027y

Reference yield: 95.0%

: 75-09-2
dichloromethane

: bromo(1,5-cyclooctadiene)methylpalladium(II)

: 455885-01-5
1-mesityl-3-(pyridin-2-yl)-1H-imidazol-3-ium bromide

: [PdMeBr(N-mesityl-N'-2-pyridylimidazolium)]*1/4CH₂Cl₂

Guidance literature:: In dichloromethane; a soln. of imidazolium compound in CH2Cl2 was added dropwise to a soln. of Pd-complex in CH2Cl2, stirred at rom temp. for 15 h with exclusion from light; filtered through Celite, volatiles were removed under reduced pressure, the solid was washed with diethyl ether and dried under vac.; elem. anal.;
DOI:10.1021/om201027y