sodium 3-(2-chlorofuro[3,2-d]pyrimidin-4-ylamino)-1H-pyrazole-5-carboxylate

Base Information

Chemical Name:sodium 3-(2-chlorofuro[3,2-d]pyrimidin-4-ylamino)-1H-pyrazole-5-carboxylate
CAS No.:1312929-44-4
Molecular Formula:C₁₀H₅ClN₅O₃*Na
Molecular Weight:301.624
Hs Code.:

Synonyms:sodium 3-(2-chlorofuro[3,2-d]pyrimidin-4-ylamino)-1H-pyrazole-5-carboxylate

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Chemical Property of sodium 3-(2-chlorofuro[3,2-d]pyrimidin-4-ylamino)-1H-pyrazole-5-carboxylate

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Technology Process of sodium 3-(2-chlorofuro[3,2-d]pyrimidin-4-ylamino)-1H-pyrazole-5-carboxylate

There total 6 articles about sodium 3-(2-chlorofuro[3,2-d]pyrimidin-4-ylamino)-1H-pyrazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1312929-43-3
methyl 3-(2-chlorofuro[3,2-d]pyrimidin-4-ylamino)-1H-pyrazole-5-carboxylate

: 1312929-44-4
sodium 3-(2-chlorofuro[3,2-d]pyrimidin-4-ylamino)-1H-pyrazole-5-carboxylate

Guidance literature:: With water; sodium hydroxide; In ethanol; for 24h; Reflux;

Reference yield:

: 956034-07-4
2,4-dichloro-furo[3,2-d]pyrimidine

: 1312929-44-4
sodium 3-(2-chlorofuro[3,2-d]pyrimidin-4-ylamino)-1H-pyrazole-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropylamine / isopropyl alcohol / 48 h / Reflux

2: sodium hydroxide; water / ethanol / 24 h / Reflux

With water; diisopropylamine; sodium hydroxide; In ethanol; isopropyl alcohol;

Reference yield:

: 956034-03-0
methyl 3-((tert-butoxycarbonyl)amino)furan-2-carboxylate

: 1312929-44-4
sodium 3-(2-chlorofuro[3,2-d]pyrimidin-4-ylamino)-1H-pyrazole-5-carboxylate

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C

2.1: dichloromethane / 0.75 h / 0 °C

2.2: 1 h / 20 °C

2.3: pH 8

3.1: sodium hydroxide; water / 5 h / Reflux

3.2: pH 4 - 5

4.1: trichlorophosphate; N,N-dimethyl-aniline / 3 h / 130 °C

5.1: diisopropylamine / isopropyl alcohol / 48 h / Reflux

6.1: sodium hydroxide; water / ethanol / 24 h / Reflux

With water; N,N-dimethyl-aniline; diisopropylamine; trifluoroacetic acid; sodium hydroxide; trichlorophosphate; In ethanol; dichloromethane; isopropyl alcohol;