N-Benzyl-N'-(3,6-dichlor-4-pyridazinylcarbonyl)-1-pyrrolidincarboxamidin

Base Information

Chemical Name:N-Benzyl-N'-(3,6-dichlor-4-pyridazinylcarbonyl)-1-pyrrolidincarboxamidin
CAS No.:118073-38-4
Molecular Formula:C₁₇H₁₇Cl₂N₅O
Molecular Weight:378.261
Hs Code.:

Synonyms:N-Benzyl-N'-(3,6-dichlor-4-pyridazinylcarbonyl)-1-pyrrolidincarboxamidin

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Chemical Property of N-Benzyl-N'-(3,6-dichlor-4-pyridazinylcarbonyl)-1-pyrrolidincarboxamidin

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Technology Process of N-Benzyl-N'-(3,6-dichlor-4-pyridazinylcarbonyl)-1-pyrrolidincarboxamidin

There total 4 articles about N-Benzyl-N'-(3,6-dichlor-4-pyridazinylcarbonyl)-1-pyrrolidincarboxamidin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 118073-12-4
N-(3,6-Dichlor-4-pyridazinylcarbonyl)-1-pyrrolidincarboximidoylchlorid

: 100-46-9
benzylamine

: 118073-38-4
N-Benzyl-N'-(3,6-dichlor-4-pyridazinylcarbonyl)-1-pyrrolidincarboxamidin

Guidance literature:: In tetrahydrofuran; for 24h; Ambient temperature;
DOI:10.1002/ardp.19883210907

Reference yield:

: 51149-08-7
3,6-dichloropyridazin-4-carboxylic acid

: 118073-38-4
N-Benzyl-N'-(3,6-dichlor-4-pyridazinylcarbonyl)-1-pyrrolidincarboxamidin

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / SOCl₂, DMF / Heating

2: 90 percent / diethyl ether / 8 h / Heating

3: 63 percent / tetrahydrofuran / 24 h / Ambient temperature

With thionyl chloride; N,N-dimethyl-formamide; In tetrahydrofuran; diethyl ether;
DOI:10.1002/ardp.19883210907

Reference yield:

: 1530-88-7
pyrrolidine-1-carbonitrile

: 118073-38-4
N-Benzyl-N'-(3,6-dichlor-4-pyridazinylcarbonyl)-1-pyrrolidincarboxamidin

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / diethyl ether / 8 h / Heating

2: 63 percent / tetrahydrofuran / 24 h / Ambient temperature

In tetrahydrofuran; diethyl ether;
DOI:10.1002/ardp.19883210907