1,3-Dimethyl-11-p-tolyl-10,11-dihydro-1H,6aH-6-oxa-9-thia-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

Base Information

Chemical Name:1,3-Dimethyl-11-p-tolyl-10,11-dihydro-1H,6aH-6-oxa-9-thia-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione
CAS No.:116316-96-2
Molecular Formula:C₁₉H₁₈N₄O₃S
Molecular Weight:382.443
Hs Code.:

Synonyms:1,3-Dimethyl-11-p-tolyl-10,11-dihydro-1H,6aH-6-oxa-9-thia-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

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Chemical Property of 1,3-Dimethyl-11-p-tolyl-10,11-dihydro-1H,6aH-6-oxa-9-thia-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

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Technology Process of 1,3-Dimethyl-11-p-tolyl-10,11-dihydro-1H,6aH-6-oxa-9-thia-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

There total 3 articles about 1,3-Dimethyl-11-p-tolyl-10,11-dihydro-1H,6aH-6-oxa-9-thia-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 116316-91-7
1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde oxime

: 116316-96-2
1,3-Dimethyl-11-p-tolyl-10,11-dihydro-1H,6aH-6-oxa-9-thia-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

Guidance literature:: With sodium hypochlorite; triethylamine; In dichloromethane; at 0 - 10 ℃; for 3h;
DOI:10.1055/s-1988-27568

Reference yield:

: 116360-56-6
1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

: 116316-96-2
1,3-Dimethyl-11-p-tolyl-10,11-dihydro-1H,6aH-6-oxa-9-thia-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NH₂OH*HCl, aq. NaOH / ethanol / 4 h / Ambient temperature

2: 78 percent / Et₃N, 10percent aq. NaOCl / CH₂Cl₂ / 3 h / 0 - 10 °C

With sodium hydroxide; sodium hypochlorite; hydroxylamine hydrochloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1055/s-1988-27568

Reference yield:

: 35824-85-2
6-chloro-5-formyl-1,3-dimethyluracil

: 116316-96-2
1,3-Dimethyl-11-p-tolyl-10,11-dihydro-1H,6aH-6-oxa-9-thia-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 12 h / Ambient temperature

2: 65 percent / NH₂OH*HCl, aq. NaOH / ethanol / 4 h / Ambient temperature

3: 78 percent / Et₃N, 10percent aq. NaOCl / CH₂Cl₂ / 3 h / 0 - 10 °C

With sodium hydroxide; sodium hypochlorite; hydroxylamine hydrochloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1055/s-1988-27568