1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

Base Information

• Chemical Name: 1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde
• CAS No.: 116360-56-6
• Molecular Formula: C₁₉H₁₉N₃O₃S
• Molecular Weight: 369.444

Synonyms:1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

Chemical Property of 1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

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Technology Process of 1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

There total 1 articles about 1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-((thiophene-2-yl)methyl)-4-methylbenzeneamine (3139-30-8) + 6-chloro-5-formyl-1,3-dimethyluracil (35824-85-2) → 1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde (116360-56-6)

Guidance literature:

With triethylamine; In dichloromethane; for 12h; Ambient temperature;

DOI:10.1055/s-1988-27568

Reference yield: 80.0%

phenylhydrazine hydrochloride (59-88-1) + 1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde (116360-56-6) → 1,3-Dimethyl-5-(phenyl-hydrazonomethyl)-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1H-pyrimidine-2,4-dione

Guidance literature:

With sodium acetate; In ethanol; 1.) 15 min, 2.) heating, 15 min;

DOI:10.1039/P19960001999

Reference yield: 65.0%

1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde (116360-56-6) → 1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde oxime (116316-91-7)

Guidance literature:

With sodium hydroxide; hydroxylamine hydrochloride; In ethanol; for 4h; Ambient temperature;

DOI:10.1055/s-1988-27568

upstream raw materials:

N-((thiophene-2-yl)methyl)-4-methylbenzeneamine

6-chloro-5-formyl-1,3-dimethyluracil

Downstream raw materials:

1,3-Dimethyl-2,4-dioxo-6-(thiophen-2-ylmethyl-p-tolyl-amino)-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde oxime

5,7-dimethyl-1-phenyl-1,7-dihydro-pyrazolo[3,4-d]pyrimidine-4,6-dione

1,3-Dimethyl-11-p-tolyl-10,11-dihydro-1H,6aH-6-oxa-9-thia-1,3,5,11-tetraaza-pentaleno[1,6a-a]naphthalene-2,4-dione

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