C₆₁H₄₃BN₂O₆

Base Information

Chemical Name:C₆₁H₄₃BN₂O₆
CAS No.:1308305-34-1
Molecular Formula:C₆₁H₄₃BN₂O₆
Molecular Weight:910.833
Hs Code.:

C<sub>61</sub>H<sub>43</sub>BN<sub>2</sub>O<sub>6</sub>

Synonyms:C₆₁H₄₃BN₂O₆

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Chemical Property of C₆₁H₄₃BN₂O₆

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Technology Process of C₆₁H₄₃BN₂O₆

There total 11 articles about C₆₁H₄₃BN₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 67-56-1
methanol

: 1308305-28-3
C₆₄H₄₈BN₃O₅

: 124-41-4
sodium methylate

: 1308305-34-1
C₆₁H₄₃BN₂O₆

Guidance literature:: C₆₄H₄₈BN₃O₅; With sulfuric acid; water; In tetrahydrofuran; at 75 ℃; for 1h;

methanol; sodium methylate; In tetrahydrofuran; at 25 ℃; for 0.166667h;
DOI:10.1021/jo200246q

Reference yield:

: 168021-39-4
C₁₇H₁₆O₄

: 1308305-34-1
C₆₁H₄₃BN₂O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: ammonium hydroxide / methanol; water; acetic acid / 24 h / 20 °C

2.1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

3.1: ethylmagnesium bromide / tetrahydrofuran / 2 h / 50 °C / Inert atmosphere

3.2: 16 h / 25 - 70 °C / Inert atmosphere

4.1: sulfuric acid; water / tetrahydrofuran / 1 h / 75 °C

4.2: 0.17 h / 25 °C

With ammonium hydroxide; sulfuric acid; boron trifluoride diethyl etherate; ethylmagnesium bromide; water; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid;
DOI:10.1021/jo200246q

Reference yield:

: C₁₇H₁₈N₂O₄

: 1308305-34-1
C₆₁H₄₃BN₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: lead(IV) tetraacetate / tetrahydrofuran / 1 h / 25 °C / Inert atmosphere

2.1: ammonium hydroxide / methanol; water; acetic acid / 24 h / 20 °C

3.1: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

4.1: ethylmagnesium bromide / tetrahydrofuran / 2 h / 50 °C / Inert atmosphere

4.2: 16 h / 25 - 70 °C / Inert atmosphere

5.1: sulfuric acid; water / tetrahydrofuran / 1 h / 75 °C

5.2: 0.17 h / 25 °C

With ammonium hydroxide; sulfuric acid; boron trifluoride diethyl etherate; ethylmagnesium bromide; water; lead(IV) tetraacetate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid;
DOI:10.1021/jo200246q