Dichlorobis(4-chlorophenoxy)methane

Base Information

• Chemical Name: Dichlorobis(4-chlorophenoxy)methane
• CAS No.: 121077-71-2
• Molecular Formula: C₁₃H₈Cl₄O₂
• Molecular Weight: 338.017

Synonyms:Dichlorobis(4-chlorophenoxy)methane

Chemical Property of Dichlorobis(4-chlorophenoxy)methane

Chemical Property:

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Technology Process of Dichlorobis(4-chlorophenoxy)methane

There total 1 articles about Dichlorobis(4-chlorophenoxy)methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

bis(p-chlorophenoxy)methane (555-89-5) → Dichlorobis(4-chlorophenoxy)methane (121077-71-2)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); chlorine; In tetrachloromethane; at 80 - 85 ℃; for 2h;

DOI:10.1055/s-1988-27765

Reference yield: 79.0%

(cyclopent-1-enylmethyl)-trimethyl-silane (75311-60-3) + Dichlorobis(4-chlorophenoxy)methane (121077-71-2) → 2-Methylene-cyclopentanecarboxylic acid 4-chloro-phenyl ester (121077-74-5)

Guidance literature:

With tin(IV) chloride; In dichloromethane; at -30 ℃; for 4h;

DOI:10.1055/s-1988-27766

Reference yield: 78.0%

Dichlorobis(4-chlorophenoxy)methane (121077-71-2) + allyl-trimethyl-silane (762-72-1) → But-3-enoic acid 4-chloro-phenyl ester (121077-72-3)

Guidance literature:

With tin(IV) chloride; In dichloromethane; at -78 ℃; for 72h;

DOI:10.1055/s-1988-27766

upstream raw materials:

bis(p-chlorophenoxy)methane

Downstream raw materials:

3-Methyl-but-3-enoic acid 4-chloro-phenyl ester

2,2-Dimethyl-but-3-enoic acid 4-chloro-phenyl ester

3-Chloro-3-methyl-2-trimethylsilanylmethyl-butyric acid 4-chloro-phenyl ester

2-Methylene-cyclohexanecarboxylic acid 4-chloro-phenyl ester

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