((2S,4S)-4-azido-2-(bis(ethylthio)methyl)pyrrolidin-1-yl)(4-(3-azidopropoxy)-5-methoxy-2-nitrophenyl)methanone

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Chemical Name:((2S,4S)-4-azido-2-(bis(ethylthio)methyl)pyrrolidin-1-yl)(4-(3-azidopropoxy)-5-methoxy-2-nitrophenyl)methanone
CAS No.:1238824-48-0
Molecular Formula:C₂₀H₂₈N₈O₅S₂
Molecular Weight:524.625
Hs Code.:

Synonyms:((2S,4S)-4-azido-2-(bis(ethylthio)methyl)pyrrolidin-1-yl)(4-(3-azidopropoxy)-5-methoxy-2-nitrophenyl)methanone

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Chemical Property of ((2S,4S)-4-azido-2-(bis(ethylthio)methyl)pyrrolidin-1-yl)(4-(3-azidopropoxy)-5-methoxy-2-nitrophenyl)methanone

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Technology Process of ((2S,4S)-4-azido-2-(bis(ethylthio)methyl)pyrrolidin-1-yl)(4-(3-azidopropoxy)-5-methoxy-2-nitrophenyl)methanone

There total 1 articles about ((2S,4S)-4-azido-2-(bis(ethylthio)methyl)pyrrolidin-1-yl)(4-(3-azidopropoxy)-5-methoxy-2-nitrophenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1238824-41-3
C₁₆H₁₈N₈O₆

: 75-08-1
ethanethiol

: 1238824-48-0
((2S,4S)-4-azido-2-(bis(ethylthio)methyl)pyrrolidin-1-yl)(4-(3-azidopropoxy)-5-methoxy-2-nitrophenyl)methanone

Guidance literature:: C₁₆H₁₈N₈O₆; ethanethiol; In dichloromethane; for 0.5h;

With chloro-trimethyl-silane; In dichloromethane; for 12h;
DOI:10.1016/j.tet.2010.05.003

Reference yield: 82.0%

: 1037070-06-6
(2S)-N-[5-methoxy-4-(2-propynyloxy)-2-nitrobenzoyl]-pyrrolidine-2-carboxaldehyde diethyl-dithioacetal

: 1238824-48-0
((2S,4S)-4-azido-2-(bis(ethylthio)methyl)pyrrolidin-1-yl)(4-(3-azidopropoxy)-5-methoxy-2-nitrophenyl)methanone

: 1238824-57-1
(4-((1-((3S,5S)-5-(bis(ethylthio)methyl)-1-(4-(3-(4-((4-((S)-2-(bis(ethylthio)methyl)pyrrolidine-1-carbonyl)-2-methoxy-5-nitro-phenoxy)methyl)-1H-1,2,3-triazol-1-yl)propoxy)-5-methoxy-2-nitro-benzoyl)pyrrolidin-3-yl)-1H-1,2,3-triazol-4-yl)methoxy)-5-methoxy-2-nitrophenyl)((S)-2-(bis(ethylthio)methyl)pyrrolidin-1-yl)methanone

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; for 12h;
DOI:10.1016/j.tet.2010.05.003