2,3-dihydroxy-5-iodobenzoic acid methyl ester

Base Information

Chemical Name:2,3-dihydroxy-5-iodobenzoic acid methyl ester
CAS No.:1056028-63-7
Molecular Formula:C₈H₇IO₄
Molecular Weight:294.046
Hs Code.:

Synonyms:2,3-dihydroxy-5-iodobenzoic acid methyl ester

Suppliers and Price of 2,3-dihydroxy-5-iodobenzoic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 16 raw suppliers

Chemical Property of 2,3-dihydroxy-5-iodobenzoic acid methyl ester

Chemical Property:

Purity/Quality:: 99% ,98%,Electron Grade , ^*data from raw suppliers

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Technology Process of 2,3-dihydroxy-5-iodobenzoic acid methyl ester

There total 3 articles about 2,3-dihydroxy-5-iodobenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 134419-44-6
methyl 5-iodo-3-methoxysalicylate

: 1056028-63-7
2,3-dihydroxy-5-iodobenzoic acid methyl ester

Guidance literature:: methyl 5-iodo-3-methoxysalicylate; With boron tribromide; In dichloromethane; water; at 20 ℃; for 1h; Inert atmosphere;

With sulfuric acid; In methanol; dichloromethane; Reflux;
DOI:10.1016/j.jinorgbio.2018.10.008

Reference yield:

: 6342-70-7
3-methoxymethylsalicylate

: 1056028-63-7
2,3-dihydroxy-5-iodobenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; silver nitrate; Iodine monochloride / chloroform

2.1: boron tribromide / dichloromethane; water / 1 h / 20 °C / Inert atmosphere

2.2: Reflux

With pyridine; Iodine monochloride; boron tribromide; silver nitrate; In dichloromethane; chloroform; water;
DOI:10.1016/j.jinorgbio.2018.10.008