(2S)-2-benzyloxycarbonylamino-4-oxo-hexanedioic acid 1-benzyl ester 6-ethyl ester

Base Information

Chemical Name:(2S)-2-benzyloxycarbonylamino-4-oxo-hexanedioic acid 1-benzyl ester 6-ethyl ester
CAS No.:754987-62-7
Molecular Formula:C₂₃H₂₅NO₇
Molecular Weight:427.454
Hs Code.:

Synonyms:(2S)-2-benzyloxycarbonylamino-4-oxo-hexanedioic acid 1-benzyl ester 6-ethyl ester

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Chemical Property of (2S)-2-benzyloxycarbonylamino-4-oxo-hexanedioic acid 1-benzyl ester 6-ethyl ester

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Technology Process of (2S)-2-benzyloxycarbonylamino-4-oxo-hexanedioic acid 1-benzyl ester 6-ethyl ester

There total 5 articles about (2S)-2-benzyloxycarbonylamino-4-oxo-hexanedioic acid 1-benzyl ester 6-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 4779-31-1
Z-Asp-OBn

: 37517-78-5
magnesium bis(3-ethoxy-3-oxopropanoate)

: 754987-62-7
(2S)-2-benzyloxycarbonylamino-4-oxo-hexanedioic acid 1-benzyl ester 6-ethyl ester

Guidance literature:: Z-Asp-OBn; With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 20 ℃; for 2h;

magnesium bis(3-ethoxy-3-oxopropanoate); In tetrahydrofuran; at 20 ℃;
DOI:10.1002/anie.200454116

Reference yield: 69.0%

: 623-73-4
diazoacetic acid ethyl ester

: 58578-45-3
(2S)-2-(benzyloxycarbonylamino)-4-oxobutyric acid benzyl ester

: 754987-62-7
(2S)-2-benzyloxycarbonylamino-4-oxo-hexanedioic acid 1-benzyl ester 6-ethyl ester

Guidance literature:: With tin(ll) chloride; In dichloromethane; at 20 - 25 ℃;
DOI:10.1039/c0ob00199f

Reference yield:

: 58578-44-2
benzyl L-2-<(carbobenzxyloxy)amino>-4-hydroxybutyrate

: 754987-62-7
(2S)-2-benzyloxycarbonylamino-4-oxo-hexanedioic acid 1-benzyl ester 6-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

2: tin(ll) chloride / dichloromethane / 0.5 h / 20 - 25 °C

With Dess-Martin periodane; tin(ll) chloride; In dichloromethane;
DOI:10.1039/c1ob05815k