(3R,4S)-3,4-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-hexanedial

Base Information

Chemical Name:(3R,4S)-3,4-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-hexanedial
CAS No.:116503-82-3
Molecular Formula:C₄₀H₅₀O₄Si₂
Molecular Weight:651.006
Hs Code.:

Synonyms:(3R,4S)-3,4-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-hexanedial

Suppliers and Price of (3R,4S)-3,4-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-hexanedial

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3R,4S)-3,4-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-hexanedial

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3R,4S)-3,4-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-hexanedial

There total 2 articles about (3R,4S)-3,4-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-hexanedial which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 116503-82-3
(3R,4S)-3,4-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-hexanedial

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / imidazole / tetrahydrofuran / 12 h

2: 1.) O₃, 2.) (MeO)3P / 1.) EtOAc-MeOH 1:1, -78 deg C, 2.) from -78 deg C to 25 deg C, 10 h

With 1H-imidazole; ozone; phosphorous acid trimethyl ester; In tetrahydrofuran;
DOI:10.1021/ja00229a068

Reference yield:

: 116503-81-2
(RS,SR)-1,2-bis[{[(1,1-dimethylethyl)diphenylsilyl]oxy}methyl]-4-cyclohexene

: 116503-82-3
(3R,4S)-3,4-Bis-(tert-butyl-diphenyl-silanyloxymethyl)-hexanedial

Guidance literature:: With ozone; phosphorous acid trimethyl ester; Multistep reaction; 1.) EtOAc-MeOH 1:1, -78 deg C, 2.) from -78 deg C to 25 deg C, 10 h;
DOI:10.1021/ja00229a068