tert-butyl (2-(2-((tert-butyldimethylsilyl)oxy)ethyl)phenoxy)dimethylsilane

Base Information

Chemical Name:tert-butyl (2-(2-((tert-butyldimethylsilyl)oxy)ethyl)phenoxy)dimethylsilane
CAS No.:160701-50-8
Molecular Formula:C₂₀H₃₈O₂Si₂
Molecular Weight:366.692
Hs Code.:

Synonyms:tert-butyl (2-(2-((tert-butyldimethylsilyl)oxy)ethyl)phenoxy)dimethylsilane

Suppliers and Price of tert-butyl (2-(2-((tert-butyldimethylsilyl)oxy)ethyl)phenoxy)dimethylsilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of tert-butyl (2-(2-((tert-butyldimethylsilyl)oxy)ethyl)phenoxy)dimethylsilane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of tert-butyl (2-(2-((tert-butyldimethylsilyl)oxy)ethyl)phenoxy)dimethylsilane

There total 3 articles about tert-butyl (2-(2-((tert-butyldimethylsilyl)oxy)ethyl)phenoxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 7768-28-7
2-(2-hydroxyphenyl)ethanol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 160701-50-8
tert-butyl (2-(2-((tert-butyldimethylsilyl)oxy)ethyl)phenoxy)dimethylsilane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/S0040-4039(00)78344-4

Reference yield:

: 614-75-5
2-Hydroxyphenylacetic acid

: 160701-50-8
tert-butyl (2-(2-((tert-butyldimethylsilyl)oxy)ethyl)phenoxy)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 1 h / 0 °C

1.2: 3 h / 0 - 20 °C

2.1: 1H-imidazole / N,N-dimethyl-formamide / 72 h / 0 - 20 °C

With 1H-imidazole; chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: C₁₁H₁₂O₅

: 160701-50-8
tert-butyl (2-(2-((tert-butyldimethylsilyl)oxy)ethyl)phenoxy)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; water / tetrahydrofuran / 3 h / 0 - 20 °C

2: 1H-imidazole / N,N-dimethyl-formamide / 72 h / 0 - 20 °C

With 1H-imidazole; sodium tetrahydroborate; water; In tetrahydrofuran; N,N-dimethyl-formamide;