(2S,4aS,7R,8aR)-[2-(3-benzyl-4,4,7-trimethyl-octahydrobenzo[e][1,3]oxazin-2-yl)benzylidene]phenyl amine

Base Information

Chemical Name:(2S,4aS,7R,8aR)-[2-(3-benzyl-4,4,7-trimethyl-octahydrobenzo[e][1,3]oxazin-2-yl)benzylidene]phenyl amine
CAS No.:865262-76-6
Molecular Formula:C₃₁H₃₆N₂O
Molecular Weight:452.64
Hs Code.:

Synonyms:(2S,4aS,7R,8aR)-[2-(3-benzyl-4,4,7-trimethyl-octahydrobenzo[e][1,3]oxazin-2-yl)benzylidene]phenyl amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,4aS,7R,8aR)-[2-(3-benzyl-4,4,7-trimethyl-octahydrobenzo[e][1,3]oxazin-2-yl)benzylidene]phenyl amine

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Technology Process of (2S,4aS,7R,8aR)-[2-(3-benzyl-4,4,7-trimethyl-octahydrobenzo[e][1,3]oxazin-2-yl)benzylidene]phenyl amine

There total 3 articles about (2S,4aS,7R,8aR)-[2-(3-benzyl-4,4,7-trimethyl-octahydrobenzo[e][1,3]oxazin-2-yl)benzylidene]phenyl amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 865262-74-4
(2S,4aS,7R,8aR)-N-benzyl-2-(o-formylphenyl)-4,4,7-trimethyl-octahydrobenzo[e][1,3]oxazine

: 62-53-3
aniline

: 865262-76-6
(2S,4aS,7R,8aR)-[2-(3-benzyl-4,4,7-trimethyl-octahydrobenzo[e][1,3]oxazin-2-yl)benzylidene]phenyl amine

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1021/jo0509509

Reference yield:

: 115156-56-4
(1R,2S,5R)-5-methyl-2-<1-methyl-1-(benzylamino)ethyl>cyclohexan-1-ol

: 865262-76-6
(2S,4aS,7R,8aR)-[2-(3-benzyl-4,4,7-trimethyl-octahydrobenzo[e][1,3]oxazin-2-yl)benzylidene]phenyl amine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / benzene / 16 h / Heating

2: 98 percent / CH₂Cl₂ / 20 °C

In dichloromethane; benzene;
DOI:10.1021/jo0509509

Reference yield:

: 643-79-8
o-phthalic dicarboxaldehyde

: 865262-76-6
(2S,4aS,7R,8aR)-[2-(3-benzyl-4,4,7-trimethyl-octahydrobenzo[e][1,3]oxazin-2-yl)benzylidene]phenyl amine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / benzene / 16 h / Heating

2: 98 percent / CH₂Cl₂ / 20 °C

In dichloromethane; benzene;
DOI:10.1021/jo0509509