2',3'-di-O-p-toluenesulfonyl-5'-O-(triphenylmethyl)-2',3'-secoadenosine

Base Information

Chemical Name:2',3'-di-O-p-toluenesulfonyl-5'-O-(triphenylmethyl)-2',3'-secoadenosine
CAS No.:104548-61-0
Molecular Formula:C₄₃H₄₁N₅O₈S₂
Molecular Weight:819.959
Hs Code.:

Synonyms:2',3'-di-O-p-toluenesulfonyl-5'-O-(triphenylmethyl)-2',3'-secoadenosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2',3'-di-O-p-toluenesulfonyl-5'-O-(triphenylmethyl)-2',3'-secoadenosine

Chemical Property:

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Technology Process of 2',3'-di-O-p-toluenesulfonyl-5'-O-(triphenylmethyl)-2',3'-secoadenosine

There total 3 articles about 2',3'-di-O-p-toluenesulfonyl-5'-O-(triphenylmethyl)-2',3'-secoadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 98-59-9
p-toluenesulfonyl chloride

: 104532-12-9
5'-O-(triphenylmethyl)-2',3'-secoadenosine

: 104548-61-0
2',3'-di-O-p-toluenesulfonyl-5'-O-(triphenylmethyl)-2',3'-secoadenosine

Guidance literature:: With pyridine; for 24h; Ambient temperature;
DOI:10.1021/jm00162a005

Reference yield:

: 18048-85-6
5'-O-(triphenylmethyl)adenosine

: 104548-61-0
2',3'-di-O-p-toluenesulfonyl-5'-O-(triphenylmethyl)-2',3'-secoadenosine

Guidance literature:: Multi-step reaction with 3 steps

1: 9.9 g / sodium periodate / methanol; H₂O / 20 h / Ambient temperature

2: 87 percent / NaBH₄ / ethanol / 2 h / Ambient temperature

3: 77 percent / pyridine / 24 h / Ambient temperature

With pyridine; sodium tetrahydroborate; sodium periodate; In methanol; ethanol; water;
DOI:10.1021/jm00162a005

Reference yield:

: 104532-11-8
(R)-2-[(R)-1-(6-Amino-purin-9-yl)-2-oxo-ethoxy]-3-trityloxy-propionaldehyde

: 104548-61-0
2',3'-di-O-p-toluenesulfonyl-5'-O-(triphenylmethyl)-2',3'-secoadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NaBH₄ / ethanol / 2 h / Ambient temperature

2: 77 percent / pyridine / 24 h / Ambient temperature

With pyridine; sodium tetrahydroborate; In ethanol;
DOI:10.1021/jm00162a005