(S)-6-(tert-Butyl-diphenyl-silanyloxy)-5-hydroxy-hexanoic acid 4-methoxy-benzyl ester

Base Information

Chemical Name:(S)-6-(tert-Butyl-diphenyl-silanyloxy)-5-hydroxy-hexanoic acid 4-methoxy-benzyl ester
CAS No.:213532-97-9
Molecular Formula:C₃₀H₃₈O₅Si
Molecular Weight:506.714
Hs Code.:

Synonyms:(S)-6-(tert-Butyl-diphenyl-silanyloxy)-5-hydroxy-hexanoic acid 4-methoxy-benzyl ester

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Chemical Property of (S)-6-(tert-Butyl-diphenyl-silanyloxy)-5-hydroxy-hexanoic acid 4-methoxy-benzyl ester

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Technology Process of (S)-6-(tert-Butyl-diphenyl-silanyloxy)-5-hydroxy-hexanoic acid 4-methoxy-benzyl ester

There total 2 articles about (S)-6-(tert-Butyl-diphenyl-silanyloxy)-5-hydroxy-hexanoic acid 4-methoxy-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 213532-96-8
(S)-5,6-Dihydroxy-hexanoic acid 4-methoxy-benzyl ester

: 213532-97-9
(S)-6-(tert-Butyl-diphenyl-silanyloxy)-5-hydroxy-hexanoic acid 4-methoxy-benzyl ester

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 12h; Ambient temperature;
DOI:10.1055/s-1998-2123

Reference yield:

: 187851-95-2
(4-methoxyphenyl)methyl hex-5-enoate

: 213532-97-9
(S)-6-(tert-Butyl-diphenyl-silanyloxy)-5-hydroxy-hexanoic acid 4-methoxy-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / 1,4-bis(dihydroquininyl)anthraquinone, K₃Fe(CN)6, K₂CO₃, NaHCO₃, potassium osmate(VI) dihydrate, H₂O / 2-methyl-propan-2-ol / 12 h / 0 °C

2: 91 percent / imidazole / dimethylformamide / 12 h / Ambient temperature

With 1H-imidazole; potassium osmate(VI); 1,4-bis(dihydroquinidinyl)anthraquinone; water; sodium hydrogencarbonate; potassium carbonate; potassium hexacyanoferrate(III); In N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1055/s-1998-2123