C₂₅H₃₁FN₂O₃

Base Information

Chemical Name:C₂₅H₃₁FN₂O₃
CAS No.:852660-64-1
Molecular Formula:C₂₅H₃₁FN₂O₃
Molecular Weight:426.531
Hs Code.:

C<sub>25</sub>H<sub>31</sub>FN<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₅H₃₁FN₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₁FN₂O₃

Chemical Property:

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Technology Process of C₂₅H₃₁FN₂O₃

There total 14 articles about C₂₅H₃₁FN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 852660-63-0
C₂₇H₃₅FN₂O₄

: 852660-64-1
C₂₅H₃₁FN₂O₃

Guidance literature:: C₂₇H₃₅FN₂O₄; With hydrogenchloride; In water; acetonitrile; at 20 ℃; for 24h;

With sodium carbonate; In water; acetonitrile;

Reference yield:

: 136265-10-6,352-03-4,24393-50-8
ethyl 4-fluorocinnamate

: 852660-64-1
C₂₅H₃₁FN₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogen / palladium 10% on activated carbon / ethanol / 2585.81 Torr

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 72 h / 0 - 20 °C

2.2: 1 h

3.1: phosphorus tribromide / chloroform / 25 °C / Heating / reflux

4.1: tetrahydrofuran / 25 °C

5.1: dichloromethane / 0.5 h / 20 °C

5.2: 16 h / 20 °C

6.1: hydrogenchloride / water; acetonitrile / 24 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen; phosphorus tribromide; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; acetonitrile;

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 852660-64-1
C₂₅H₃₁FN₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene / Heating / reflux

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 2585.81 Torr

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 72 h / 0 - 20 °C

3.2: 1 h

4.1: phosphorus tribromide / chloroform / 25 °C / Heating / reflux

5.1: tetrahydrofuran / 25 °C

6.1: dichloromethane / 0.5 h / 20 °C

6.2: 16 h / 20 °C

7.1: hydrogenchloride / water; acetonitrile / 24 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen; phosphorus tribromide; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; toluene; acetonitrile;