BENZYL 2-ACETAMIDO-2-DEOXY-4,6-O-ISOPROPYLIDENE-D-GALACTOPYRANOSIDE

Base Information

• Chemical Name: BENZYL 2-ACETAMIDO-2-DEOXY-4,6-O-ISOPROPYLIDENE-D-GALACTOPYRANOSIDE
• CAS No.: 75263-33-1
• Molecular Formula: C18H25 N O6
• Molecular Weight: 351.397
• Mol file: 75263-33-1.mol

Synonyms:Pyrano[3,2-d]-1,3-dioxin,a-D-galactopyranoside deriv.

Chemical Property of BENZYL 2-ACETAMIDO-2-DEOXY-4,6-O-ISOPROPYLIDENE-D-GALACTOPYRANOSIDE

Chemical Property:

• PSA: 86.25000
• LogP: 1.33610

Purity/Quality:

95% ^*data from raw suppliers

Benzyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-D-galactopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZYL 2-ACETAMIDO-2-DEOXY-4,6-O-ISOPROPYLIDENE-D-GALACTOPYRANOSIDE

There total 3 articles about BENZYL 2-ACETAMIDO-2-DEOXY-4,6-O-ISOPROPYLIDENE-D-GALACTOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

benzyl 2-acetamido-2-deoxy-α-D-galactopyranoside (3554-93-6,347411-88-5) + 2,2-dimethoxy-propane (77-76-9) → benzyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-α-D-galactopyranoside (75263-33-1) + benzyl 2-acetamido-2-deoxy-3,4-O-isopropylidene-α-D-galactopyranoside (112289-51-7)

Guidance literature:

With camphor-10-sulfonic acid; for 48h; Ambient temperature;

DOI:10.1016/S0008-6215(97)10017-9

Reference yield: 78.0%

benzyl 2-acetamido-2-deoxy-α-D-galactopyranoside (3554-93-6,347411-88-5) + 2,2-dimethoxy-propane (77-76-9) → benzyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-α-D-galactopyranoside (75263-33-1)

Guidance literature:

With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; for 1.5h; Ambient temperature;

DOI:10.1016/S0008-6215(00)80713-2

Reference yield:

benzyl 2-acetamido-2-deoxy-3,6-di-O-pivaloyl-α-D-glucopyranoside (206751-88-4) → benzyl 2-acetamido-2-deoxy-4,6-O-isopropylidene-α-D-galactopyranoside (75263-33-1)

Guidance literature:

Multi-step reaction with 2 steps

2: (+/-)-camphor-10-sulfonic acid / 48 h / Ambient temperature

With camphor-10-sulfonic acid;

DOI:10.1016/S0008-6215(97)10017-9

upstream raw materials:

benzyl 2-acetamido-2-deoxy-α-D-galactopyranoside

2,2-dimethoxy-propane

benzyl 2-acetamido-2-deoxy-3,6-di-O-pivaloyl-α-D-glucopyranoside

Downstream raw materials:

benzyl 2-acetamido-3-O-(D-1-carboxyethyl)-2-deoxy-α-D-galactopyranoside

2-((4aR,6S,7R,8R,8aR)-7-Acetylamino-6-benzyloxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-propionic acid

benzyl 2-acetamido-4,6-di-O-acetyl-2-deoxy-3-O--α-D-galactopyranoside

benzyl 2-acetamido-3-O-acetyl-2-deoxy-4,6-O-isopropylidene-α-D-galactopyranoside

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