Technology Process of C17H24O5
There total 5 articles about C17H24O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydride / tetrahydrofuran / 3 h / 0 - 20 °C
2: potassium osmate(VI) dihydrate; (DHQD)2PHAL; methanesulfonamide; K3[Fe(CN)6]; potassium carbonate / water; tert-butyl alcohol / 24 h / 0 °C
3: toluene-4-sulfonic acid / acetone / 12 h / 20 °C
With
potassium osmate(VI) dihydrate; (DHQD)2PHAL; methanesulfonamide; K3[Fe(CN)6]; sodium hydride; potassium carbonate; toluene-4-sulfonic acid;
In
tetrahydrofuran; water; acetone; tert-butyl alcohol;
1: Horner-Wittig olefination;
DOI:10.1016/j.tetlet.2011.02.014
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 12 h / 0 - 20 °C
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.17 h / -78 °C
2.2: 0.75 h
2.3: 1.5 h / -78 - 20 °C
3.1: sodium hydride / tetrahydrofuran / 3 h / 0 - 20 °C
4.1: potassium osmate(VI) dihydrate; (DHQD)2PHAL; methanesulfonamide; K3[Fe(CN)6]; potassium carbonate / water; tert-butyl alcohol / 24 h / 0 °C
5.1: toluene-4-sulfonic acid / acetone / 12 h / 20 °C
With
potassium osmate(VI) dihydrate; (DHQD)2PHAL; oxalyl dichloride; methanesulfonamide; K3[Fe(CN)6]; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide;
In
tetrahydrofuran; dichloromethane; water; acetone; tert-butyl alcohol;
2.1: Swern oxidation / 2.2: Swern oxidation / 2.3: Swern oxidation / 3.1: Horner-Wittig olefination;
DOI:10.1016/j.tetlet.2011.02.014