3-phenyl-5-trifluoromethyl-2,2,2-tris(4-methylphenoxy)-2,3-dihydro-1,3,4,2-oxadiazaphosphole

Base Information

Chemical Name:3-phenyl-5-trifluoromethyl-2,2,2-tris(4-methylphenoxy)-2,3-dihydro-1,3,4,2-oxadiazaphosphole
CAS No.:86508-64-7
Molecular Formula:C₂₉H₂₆F₃N₂O₄P
Molecular Weight:554.505
Hs Code.:

Synonyms:3-phenyl-5-trifluoromethyl-2,2,2-tris(4-methylphenoxy)-2,3-dihydro-1,3,4,2-oxadiazaphosphole

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Chemical Property of 3-phenyl-5-trifluoromethyl-2,2,2-tris(4-methylphenoxy)-2,3-dihydro-1,3,4,2-oxadiazaphosphole

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Technology Process of 3-phenyl-5-trifluoromethyl-2,2,2-tris(4-methylphenoxy)-2,3-dihydro-1,3,4,2-oxadiazaphosphole

There total 2 articles about 3-phenyl-5-trifluoromethyl-2,2,2-tris(4-methylphenoxy)-2,3-dihydro-1,3,4,2-oxadiazaphosphole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34064-31-8
2,2,2-trifluoro-N′-phenylacetohydrazide

: 86508-64-7
3-phenyl-5-trifluoromethyl-2,2,2-tris(4-methylphenoxy)-2,3-dihydro-1,3,4,2-oxadiazaphosphole

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / PCl₅ / toluene / 2 h / Ambient temperature

2: 54 percent / toluene / 4.5 h / Heating

With phosphorus pentachloride; In toluene;
DOI:10.1246/bcsj.57.2689

Reference yield:

: 100-63-0
phenylhydrazine

: 86508-64-7
3-phenyl-5-trifluoromethyl-2,2,2-tris(4-methylphenoxy)-2,3-dihydro-1,3,4,2-oxadiazaphosphole

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent

2: 93 percent / PCl₅ / toluene / 2 h / Ambient temperature

3: 54 percent / toluene / 4.5 h / 110 °C

With phosphorus pentachloride; In toluene;
DOI:10.1246/cl.1983.507