methyl rac-(E,R)-2-(phenylselenyl)-3,4-bis(methoxycarbonyl)-3-hexadecenoate

Base Information

Chemical Name:methyl rac-(E,R)-2-(phenylselenyl)-3,4-bis(methoxycarbonyl)-3-hexadecenoate
CAS No.:1194525-28-4
Molecular Formula:C₂₇H₄₀O₆Se
Molecular Weight:539.571
Hs Code.:

Synonyms:methyl rac-(E,R)-2-(phenylselenyl)-3,4-bis(methoxycarbonyl)-3-hexadecenoate

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Chemical Property of methyl rac-(E,R)-2-(phenylselenyl)-3,4-bis(methoxycarbonyl)-3-hexadecenoate

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Technology Process of methyl rac-(E,R)-2-(phenylselenyl)-3,4-bis(methoxycarbonyl)-3-hexadecenoate

There total 1 articles about methyl rac-(E,R)-2-(phenylselenyl)-3,4-bis(methoxycarbonyl)-3-hexadecenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 5927-18-4
trimethyl phosphonoacetate

: 1194525-27-3
methyl rac-(R)-3-(phenylselenyl)-3-(methoxycarbonyl)-2-oxopentadecanoate

: 1194525-31-9
methyl (Z)-3,4-bis(methoxycarbonyl)-3-hexadecenoate

: 1194525-28-4
methyl rac-(E,R)-2-(phenylselenyl)-3,4-bis(methoxycarbonyl)-3-hexadecenoate

Guidance literature:: trimethyl phosphonoacetate; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.166667h;

methyl rac-(R)-3-(phenylselenyl)-3-(methoxycarbonyl)-2-oxopentadecanoate; In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield:

: 1194525-28-4
methyl rac-(E,R)-2-(phenylselenyl)-3,4-bis(methoxycarbonyl)-3-hexadecenoate

: 136266-35-8
rac-(3S,4S,5R)-3,4-dihydroxy-5-dodecyl-4,5-dicarboxytetrahydro-2-furanone

: 136266-37-0
rac-(3R,4S,5S)-3,4-dihydroxy-3-dodecyl-4,5-dicarboxytetrahydro-2-furanone

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; dihydrogen peroxide / dichloromethane; water / 24 h / 20 °C

2: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; tert-butyl alcohol; acetone / 48 h / 20 °C

3: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C

With pyridine; osmium(VIII) oxide; water; dihydrogen peroxide; 4-methylmorpholine N-oxide; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; acetone; tert-butyl alcohol;