methyl rac-(R)-3-(phenylselenyl)-3-(methoxycarbonyl)-2-oxopentadecanoate

Base Information

Chemical Name:methyl rac-(R)-3-(phenylselenyl)-3-(methoxycarbonyl)-2-oxopentadecanoate
CAS No.:1194525-27-3
Molecular Formula:C₂₄H₃₆O₅Se
Molecular Weight:483.507
Hs Code.:

Synonyms:methyl rac-(R)-3-(phenylselenyl)-3-(methoxycarbonyl)-2-oxopentadecanoate

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Chemical Property of methyl rac-(R)-3-(phenylselenyl)-3-(methoxycarbonyl)-2-oxopentadecanoate

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Technology Process of methyl rac-(R)-3-(phenylselenyl)-3-(methoxycarbonyl)-2-oxopentadecanoate

There total 2 articles about methyl rac-(R)-3-(phenylselenyl)-3-(methoxycarbonyl)-2-oxopentadecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 34837-55-3
Phenylselenyl bromide

: methyl rac-(S)-3-(methoxycarbonyl)-2-oxopentadecanoate

: 1194525-27-3
methyl rac-(R)-3-(phenylselenyl)-3-(methoxycarbonyl)-2-oxopentadecanoate

Guidance literature:: methyl rac-(S)-3-(methoxycarbonyl)-2-oxopentadecanoate; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.166667h;

Phenylselenyl bromide; In tetrahydrofuran; at 0 - 20 ℃; for 24h;

Reference yield:

: 124-10-7
methyl myristoate

: 1194525-27-3
methyl rac-(R)-3-(phenylselenyl)-3-(methoxycarbonyl)-2-oxopentadecanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; methanol / 3 h / 20 °C / Reflux

2.1: morpholine / dichloromethane / 0.25 h / 20 °C

2.2: 24 h / 20 °C

With morpholine; sodium hydride; In tetrahydrofuran; methanol; dichloromethane;

Reference yield: 51.0%

: 5927-18-4
trimethyl phosphonoacetate

: 1194525-27-3
methyl rac-(R)-3-(phenylselenyl)-3-(methoxycarbonyl)-2-oxopentadecanoate

: 1194525-31-9
methyl (Z)-3,4-bis(methoxycarbonyl)-3-hexadecenoate

: 1194525-28-4
methyl rac-(E,R)-2-(phenylselenyl)-3,4-bis(methoxycarbonyl)-3-hexadecenoate

Guidance literature:: trimethyl phosphonoacetate; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.166667h;

methyl rac-(R)-3-(phenylselenyl)-3-(methoxycarbonyl)-2-oxopentadecanoate; In tetrahydrofuran; at 20 ℃; for 24h;