2-((Z)-5-(4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzylidene)-4-oxo-2-thioxothiazolidin-3-yl)acetic acid

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Chemical Name:2-((Z)-5-(4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzylidene)-4-oxo-2-thioxothiazolidin-3-yl)acetic acid
CAS No.:1342231-19-9
Molecular Formula:C₃₅H₂₈N₆O₃S₂
Molecular Weight:644.778
Hs Code.:

Synonyms:2-((Z)-5-(4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzylidene)-4-oxo-2-thioxothiazolidin-3-yl)acetic acid

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Chemical Property of 2-((Z)-5-(4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzylidene)-4-oxo-2-thioxothiazolidin-3-yl)acetic acid

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Technology Process of 2-((Z)-5-(4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzylidene)-4-oxo-2-thioxothiazolidin-3-yl)acetic acid

There total 2 articles about 2-((Z)-5-(4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzylidene)-4-oxo-2-thioxothiazolidin-3-yl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 5718-83-2
rhodanine 3-acetic acid

: 1342231-07-5
4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzaldehyde

: 1342231-19-9
2-((Z)-5-(4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzylidene)-4-oxo-2-thioxothiazolidin-3-yl)acetic acid

Guidance literature:: With ammonium acetate; acetic acid; for 5h; Reflux;
DOI:10.1016/j.tetlet.2011.09.116

Reference yield:

: 1342231-05-3
4-(4-chloro-6-(dimethylamino)-1,3,5-triazin-2-yl)-benzaldehyde

: 1342231-19-9
2-((Z)-5-(4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzylidene)-4-oxo-2-thioxothiazolidin-3-yl)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / 1,4-dioxane; water / 5 h / 100 °C / Inert atmosphere

2: ammonium acetate; acetic acid / 5 h / Reflux

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; ammonium acetate; potassium carbonate; acetic acid; In 1,4-dioxane; water; 1: Suzuki coupling / 2: Knoevenagel reaction;
DOI:10.1016/j.tetlet.2011.09.116