4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzaldehyde

Base Information

• Chemical Name: 4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzaldehyde
• CAS No.: 1342231-07-5
• Molecular Formula: C₃₀H₂₅N₅O
• Molecular Weight: 471.561

Synonyms:4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzaldehyde

Chemical Property of 4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzaldehyde

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Technology Process of 4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzaldehyde

There total 1 articles about 4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

4-(4-chloro-6-(dimethylamino)-1,3,5-triazin-2-yl)-benzaldehyde (1342231-05-3) + 4-(diphenylamino)phenyl boronic acid (201802-67-7) → 4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzaldehyde (1342231-07-5)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In 1,4-dioxane; water; at 100 ℃; for 5h; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.09.116

Reference yield: 85.0%

4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzaldehyde (1342231-07-5) + cyanoacetic acid (372-09-8) → (E)-3-(4-(4-(4-(diphenylamino)phenyl)-6-(dimethyl-amino)-1,3,5-triazin-2-yl)phenyl)-2-cyanoacrylic acid (1342231-16-6)

Guidance literature:

With ammonium acetate; acetic acid; for 12h; Reflux;

DOI:10.1016/j.tetlet.2011.09.116

Reference yield: 68.0%

rhodanine 3-acetic acid (5718-83-2) + 4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzaldehyde (1342231-07-5) → 2-((Z)-5-(4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzylidene)-4-oxo-2-thioxothiazolidin-3-yl)acetic acid (1342231-19-9)

Guidance literature:

With ammonium acetate; acetic acid; for 5h; Reflux;

DOI:10.1016/j.tetlet.2011.09.116

upstream raw materials:

4-(4-chloro-6-(dimethylamino)-1,3,5-triazin-2-yl)-benzaldehyde

4-(diphenylamino)phenyl boronic acid

Downstream raw materials:

2-((Z)-5-(4-(4-(4-(diphenylamino)phenyl)-6-(dimethylamino)-1,3,5-triazin-2-yl)benzylidene)-4-oxo-2-thioxothiazolidin-3-yl)acetic acid

(E)-3-(4-(4-(4-(diphenylamino)phenyl)-6-(dimethyl-amino)-1,3,5-triazin-2-yl)phenyl)-2-cyanoacrylic acid

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