N-benzyl-N-cyclohexylformamide

Base Information

• Chemical Name: N-benzyl-N-cyclohexylformamide
• CAS No.: 22779-86-8
• Molecular Formula: C₁₄H₁₉NO
• Molecular Weight: 217.311
• Mol file: 22779-86-8.mol

Synonyms:N-benzyl-N-cyclohexylformamide

Chemical Property of N-benzyl-N-cyclohexylformamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of N-benzyl-N-cyclohexylformamide

There total 3 articles about N-benzyl-N-cyclohexylformamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

formic acid (64-18-6) + iodobenzene (591-50-4) + carbon monoxide (201230-82-2) + cyclohexylamine (108-91-8,157973-60-9) → N-benzyl-N-cyclohexylformamide (22779-86-8)

Guidance literature:

With palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; In toluene; acetonitrile; at 120 ℃; for 24h; under 1500.15 Torr; Inert atmosphere;

DOI:10.1002/adsc.201800674

Reference yield:

N-benzylcyclohexylamine (4383-25-9) → N-benzyl-N-cyclohexylformamide (22779-86-8)

Guidance literature:

With dicobalt octacarbonyl; benzene; at 230 ℃; under 102971 Torr;

Reference yield:

→ N-benzyl-N-cyclohexylformamide (22779-86-8)

Guidance literature:

Benzyl-cyclohexylamin, CO Co2(CO)8, Benzol, 230grad/140 at>;

DOI:10.1246/bcsj.33.247

upstream raw materials:

N-benzylcyclohexylamine

formic acid

iodobenzene

carbon monoxide

Refernces