methyl N³-(2-benzylaminoethyl)-N²-tert-butoxycarbonyl-N³-methyl-2,3-diaminopropionate

Base Information

• Chemical Name: methyl N³-(2-benzylaminoethyl)-N²-tert-butoxycarbonyl-N³-methyl-2,3-diaminopropionate
• CAS No.: 166047-31-0
• Molecular Formula: C₁₉H₃₁N₃O₄
• Molecular Weight: 365.473

Synonyms:methyl N³-(2-benzylaminoethyl)-N²-tert-butoxycarbonyl-N³-methyl-2,3-diaminopropionate

Chemical Property of methyl N³-(2-benzylaminoethyl)-N²-tert-butoxycarbonyl-N³-methyl-2,3-diaminopropionate

Chemical Property:

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Technology Process of methyl N³-(2-benzylaminoethyl)-N²-tert-butoxycarbonyl-N³-methyl-2,3-diaminopropionate

There total 1 articles about methyl N³-(2-benzylaminoethyl)-N²-tert-butoxycarbonyl-N³-methyl-2,3-diaminopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

methyl 2-[(tert-butoxycarbonyl)amino]acrylate (55477-80-0) + N-methyl-2-(benzylamino)ethylamine (56904-09-7) → methyl N3-(2-benzylaminoethyl)-N2-tert-butoxycarbonyl-N3-methyl-2,3-diaminopropionate (166047-31-0)

Guidance literature:

for 16h; Ambient temperature;

DOI:10.1002/jhet.5570320244

Reference yield: 50.0%

methanol (67-56-1) + methyl N3-(2-benzylaminoethyl)-N2-tert-butoxycarbonyl-N3-methyl-2,3-diaminopropionate (166047-31-0) → 1-benzyl-6-methoxycarbonylamino-4-methylhexahydro-1H-1,4-diazepin-7-one + 1-benzyl-6-(tert-butoxycarbonylamino)-4-methylhexahydro-1H-1,4-diazepin-7-one

Guidance literature:

With sodium methylate; In toluene; at 80 ℃; for 2h;

DOI:10.1002/jhet.5570320244

Reference yield: 22.0%

methyl N3-(2-benzylaminoethyl)-N2-tert-butoxycarbonyl-N3-methyl-2,3-diaminopropionate (166047-31-0) → 1-benzyl-6-methoxycarbonylamino-4-methylhexahydro-1H-1,4-diazepin-7-one + 1-benzyl-6-(tert-butoxycarbonylamino)-4-methylhexahydro-1H-1,4-diazepin-7-one

Guidance literature:

With sodium methylate; In methanol; toluene; at 80 ℃; for 2h;

DOI:10.1002/jhet.5570320244

upstream raw materials:

methyl 2-[(tert-butoxycarbonyl)amino]acrylate

N-methyl-2-(benzylamino)ethylamine

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