(+/-)-phenyl (5-cyano-1-((2,4-dimethoxyphenyl)sulfonyl)-3-(2-ethoxypyridin-3-yl)-2-oxoindolin-3-yl)carbamate

Base Information

• Chemical Name: (+/-)-phenyl (5-cyano-1-((2,4-dimethoxyphenyl)sulfonyl)-3-(2-ethoxypyridin-3-yl)-2-oxoindolin-3-yl)carbamate
• CAS No.: 1037238-20-2
• Molecular Formula: C₃₁H₂₆N₄O₈S
• Molecular Weight: 614.635

Synonyms:(+/-)-phenyl (5-cyano-1-((2,4-dimethoxyphenyl)sulfonyl)-3-(2-ethoxypyridin-3-yl)-2-oxoindolin-3-yl)carbamate

Chemical Property of (+/-)-phenyl (5-cyano-1-((2,4-dimethoxyphenyl)sulfonyl)-3-(2-ethoxypyridin-3-yl)-2-oxoindolin-3-yl)carbamate

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Technology Process of (+/-)-phenyl (5-cyano-1-((2,4-dimethoxyphenyl)sulfonyl)-3-(2-ethoxypyridin-3-yl)-2-oxoindolin-3-yl)carbamate

There total 1 articles about (+/-)-phenyl (5-cyano-1-((2,4-dimethoxyphenyl)sulfonyl)-3-(2-ethoxypyridin-3-yl)-2-oxoindolin-3-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-amino-1-(2,4-dimethoxyphenylsulfonyl)-3-(2-ethoxypyridin-3-yl)-2-oxoindoline-5-carbonitrile (1037238-19-9) + phenyl chloroformate (1885-14-9) → (+/-)-phenyl (5-cyano-1-((2,4-dimethoxyphenyl)sulfonyl)-3-(2-ethoxypyridin-3-yl)-2-oxoindolin-3-yl)carbamate (1037238-20-2)

Guidance literature:

With pyridine; In dichloromethane; at 5 - 25 ℃; for 17h;

Reference yield: 21.0%

(+/-)-phenyl (5-cyano-1-((2,4-dimethoxyphenyl)sulfonyl)-3-(2-ethoxypyridin-3-yl)-2-oxoindolin-3-yl)carbamate (1037238-20-2) + 1-(1-methyl-piperidin-4-yl)-piperazine (23995-88-2) → N-[5-cyano-1-[(2,4-dimethoxyphenyl)sulphonyl]-3-(2-ethoxypyridin-3-yl)-2-oxo-2,3-dihydro-1H-indol-3-yl]-4-(1-methylpiperidin-4-yl)piperazine-1-carboxamide (1037238-62-2,1037238-60-0,1037238-14-4)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 24h;

Reference yield:

(+/-)-phenyl (5-cyano-1-((2,4-dimethoxyphenyl)sulfonyl)-3-(2-ethoxypyridin-3-yl)-2-oxoindolin-3-yl)carbamate (1037238-20-2) + 2-(1-methylpiperidin-4-yl)-2,6-diazaspiro[3.3]heptane trihydrochloride → (+/-)-N-[5-cyano-1-(2,4-dimethoxyphenyl)sulfonyl-3-(2-ethoxy-3-pyridyl)-2-oxo-indolin-3-yl]-2-(1-methyl-4-piperidyl)-2,6-diazaspiro[3.3]heptane-6-carboxamide

Guidance literature:

With triethylamine; In tetrahydrofuran; at 20 - 25 ℃; for 12h;

upstream raw materials:

3-amino-1-(2,4-dimethoxyphenylsulfonyl)-3-(2-ethoxypyridin-3-yl)-2-oxoindoline-5-carbonitrile

phenyl chloroformate

Downstream raw materials:

N-[5-cyano-1-[(2,4-dimethoxyphenyl)sulphonyl]-3-(2-ethoxypyridin-3-yl)-2-oxo-2,3-dihydro-1H-indol-3-yl]-4-(1-methylpiperidin-4-yl)piperazine-1-carboxamide

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