Technology Process of 2,4,6-Trimethoxy-3-methylphenol
There total 5 articles about 2,4,6-Trimethoxy-3-methylphenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanol; Methyl formate; copper(l) chloride;
at 115 ℃;
for 2h;
Autoclave;
Green chemistry;
DOI:10.1007/s11164-014-1917-x
- Guidance literature:
-
With
3,3-dimethyldioxirane;
In
acetone;
at -15 ℃;
for 0.5h;
DOI:10.1055/s-1994-25523
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 36.9 g / phosphoryl chloride / 1.5 h / Ambient temperature
2: 21.3 g / zinc amalgam, hydrochloric acid / acetic acid; H2O / 2 h / Heating
3: 18.0 g / phosphoryl chloride / 1.5 h / Ambient temperature
4: 1.) m-chloroperbenzoic acid, 2.) potassium hydroxide / 1.) dichloromethane, room temperature, 2.) aqueous methanol, 0 deg C, 1 h
With
hydrogenchloride; potassium hydroxide; amalgamated zinc; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate;
In
water; acetic acid;
