1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2,4(3H)-dione

Base Information

• Chemical Name: 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2,4(3H)-dione
• CAS No.: 107711-22-8
• Molecular Formula: C₃₁H₂₈N₂O₉
• Molecular Weight: 572.571

Synonyms:1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2,4(3H)-dione

Chemical Property of 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2,4(3H)-dione

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2,4(3H)-dione

There total 2 articles about 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2,4(3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

benzeneseleninic anhydride (17697-12-0) + 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2-one (77249-70-8) → 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2,4(3H)-dione (107711-22-8) + C37H32N2O9Se (107711-23-9,107711-24-0)

Guidance literature:

In toluene; for 1h; Heating;

DOI:10.1021/jo00386a015

Reference yield:

2,3,5-tri-O-benzoyl-D-ribofuranosyl bromide (22860-91-9) + tetrahydro-2H-1,3-diazepine-2,4(3H)-dione (75548-99-1) → 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2,4(3H)-dione (107711-22-8) + 3-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2,4(3H)-dione (107711-25-1)

Guidance literature:

With bis(trimethylsilyl)trifluoroacetamide; mercury dibromide; mercury(II) oxide; Yield given. Multistep reaction. Yields of byproduct given; 1.) acetonitrile, RT, 0.5 h, 2.) benzene, reflux, 18 h;

DOI:10.1021/jo00386a015

Reference yield: 65.0%

1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2,4(3H)-dione (107711-22-8) → 1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4-thioxohexahydro-2H-1,3-diazepin-2-one (107711-31-9)

Guidance literature:

With 2,4-bis(4-methoxyphenyl)-1,3-dithia-2,4-diphosphetane; In benzene; for 1h; Heating;

DOI:10.1021/jo00386a015

upstream raw materials:

benzeneseleninic anhydride

1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)tetrahydro-2H-1,3-diazepine-2-one

2,3,5-tri-O-benzoyl-D-ribofuranosyl bromide

tetrahydro-2H-1,3-diazepine-2,4(3H)-dione

Downstream raw materials:

1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4-thioxohexahydro-2H-1,3-diazepin-2-one

1-β-D-ribofuranosyl-4-aminotetrahydro-2H-1,3-diazepin-2-one

1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-4-(methylthio)tetrahydro-2H-1,3-diazepin-2-one

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