1-(1-benzyl-4-(3,5-difluoro-4'-methoxy-[1,1'-biphenyl]-4-yl)-2-methyl-1H-pyrrol-3-yl)ethanone

Base Information

Chemical Name:1-(1-benzyl-4-(3,5-difluoro-4'-methoxy-[1,1'-biphenyl]-4-yl)-2-methyl-1H-pyrrol-3-yl)ethanone
CAS No.:1318763-72-2
Molecular Formula:C₂₇H₂₃F₂NO₂
Molecular Weight:431.482
Hs Code.:

Synonyms:1-(1-benzyl-4-(3,5-difluoro-4'-methoxy-[1,1'-biphenyl]-4-yl)-2-methyl-1H-pyrrol-3-yl)ethanone

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Chemical Property of 1-(1-benzyl-4-(3,5-difluoro-4'-methoxy-[1,1'-biphenyl]-4-yl)-2-methyl-1H-pyrrol-3-yl)ethanone

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Technology Process of 1-(1-benzyl-4-(3,5-difluoro-4'-methoxy-[1,1'-biphenyl]-4-yl)-2-methyl-1H-pyrrol-3-yl)ethanone

There total 1 articles about 1-(1-benzyl-4-(3,5-difluoro-4'-methoxy-[1,1'-biphenyl]-4-yl)-2-methyl-1H-pyrrol-3-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 537013-51-7
4-bromo-2,6-difluorobenzaldehyde

: 75-52-5
nitromethane

: 5720-07-0
4-methoxyphenylboronic acid

: 123-54-6,81235-32-7
acetylacetone

: 100-46-9
benzylamine

: 1318763-72-2
1-(1-benzyl-4-(3,5-difluoro-4'-methoxy-[1,1'-biphenyl]-4-yl)-2-methyl-1H-pyrrol-3-yl)ethanone

Guidance literature:: 4-bromo-2,6-difluorobenzaldehyde; nitromethane; acetylacetone; benzylamine; With bis-triphenylphosphine-palladium(II) chloride; at 80 - 85 ℃; for 4h; Inert atmosphere; Neat (no solvent);

4-methoxyphenylboronic acid; With potassium carbonate; In 1,4-dioxane; water; at 80 - 85 ℃; for 5h; Inert atmosphere;
DOI:10.1039/c1cc12321a

Reference yield: 87.0%

: 1318763-72-2
1-(1-benzyl-4-(3,5-difluoro-4'-methoxy-[1,1'-biphenyl]-4-yl)-2-methyl-1H-pyrrol-3-yl)ethanone

: 1318763-73-3
(E)-1-(1-benzyl-4-(3,5-difluoro-4'-methoxy-[1,1'-biphenyl]-4-yl)-2-methyl-1H-pyrrol-3-yl)ethanone oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; at 20 - 85 ℃; for 3.25h; Inert atmosphere;
DOI:10.1039/c1cc12321a