Technology Process of C24H28F2O4
There total 8 articles about C24H28F2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
di-isopropyl azodicarboxylate;
In
tetrahydrofuran;
for 18h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: trifluoroacetic acid / Reflux
2: potassium carbonate / N,N-dimethyl-formamide / 50 °C
3: tetrahydrofuran / 2 h / Reflux
4: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C
5: di-isopropyl azodicarboxylate / tetrahydrofuran / 18 h
With
di-isopropyl azodicarboxylate; hydrogen; potassium carbonate; trifluoroacetic acid;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / 50 °C
2: tetrahydrofuran / 2 h / Reflux
3: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C
4: di-isopropyl azodicarboxylate / tetrahydrofuran / 18 h
With
di-isopropyl azodicarboxylate; hydrogen; potassium carbonate;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;