2-Benzyl-8a-methoxy-6,7,8,8a-tetrahydro-2H-pyrido[3,4-b]pyrrolizine-1,9-dione

Base Information

Chemical Name:2-Benzyl-8a-methoxy-6,7,8,8a-tetrahydro-2H-pyrido[3,4-b]pyrrolizine-1,9-dione
CAS No.:159791-33-0
Molecular Formula:C₁₈H₁₈N₂O₃
Molecular Weight:310.353
Hs Code.:

Synonyms:2-Benzyl-8a-methoxy-6,7,8,8a-tetrahydro-2H-pyrido[3,4-b]pyrrolizine-1,9-dione

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Chemical Property of 2-Benzyl-8a-methoxy-6,7,8,8a-tetrahydro-2H-pyrido[3,4-b]pyrrolizine-1,9-dione

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Technology Process of 2-Benzyl-8a-methoxy-6,7,8,8a-tetrahydro-2H-pyrido[3,4-b]pyrrolizine-1,9-dione

There total 10 articles about 2-Benzyl-8a-methoxy-6,7,8,8a-tetrahydro-2H-pyrido[3,4-b]pyrrolizine-1,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 67-56-1
methanol

: 159791-30-7
Trifluoro-methanesulfonic acid 2-benzyl-1-oxo-2,6,7,8-tetrahydro-1H-pyrido[3,4-b]pyrrolizin-9-yl ester

: 159791-33-0
2-Benzyl-8a-methoxy-6,7,8,8a-tetrahydro-2H-pyrido[3,4-b]pyrrolizine-1,9-dione

Guidance literature:: In dimethyl sulfoxide; at 70 ℃;
DOI:10.1021/jo00122a009

Reference yield: 65.0%

: 67-56-1
methanol

: 201230-82-2
carbon monoxide

: 159791-30-7
Trifluoro-methanesulfonic acid 2-benzyl-1-oxo-2,6,7,8-tetrahydro-1H-pyrido[3,4-b]pyrrolizin-9-yl ester

: 2-Benzyl-1-oxo-2,6,7,8-tetrahydro-1H-pyrido[3,4-b]pyrrolizine-9-carboxylic acid methyl ester

: 159791-33-0
2-Benzyl-8a-methoxy-6,7,8,8a-tetrahydro-2H-pyrido[3,4-b]pyrrolizine-1,9-dione

Guidance literature:: With palladium diacetate; triethylamine; triphenylphosphine; In dimethyl sulfoxide; at 68 ℃; for 2h;
DOI:10.1016/0040-4039(94)88205-3

Reference yield:

: 67-56-1
methanol

: 159791-30-7
Trifluoro-methanesulfonic acid 2-benzyl-1-oxo-2,6,7,8-tetrahydro-1H-pyrido[3,4-b]pyrrolizin-9-yl ester

: 2-Benzyl-1-oxo-2,6,7,8-tetrahydro-1H-pyrido[3,4-b]pyrrolizine-9-carboxylic acid methyl ester

: 159791-33-0
2-Benzyl-8a-methoxy-6,7,8,8a-tetrahydro-2H-pyrido[3,4-b]pyrrolizine-1,9-dione

Guidance literature:: With palladium diacetate; carbon monoxide; triethylamine; triphenylphosphine; In dimethyl sulfoxide; at 68 ℃; for 4h;
DOI:10.1016/0040-4039(94)88205-3