3,6-di(p-(phenylacetoxy)phenyl)-1,2,4,5-tetrakis((benzyloxy)methoxy)benzene

Base Information

Chemical Name:3,6-di(p-(phenylacetoxy)phenyl)-1,2,4,5-tetrakis((benzyloxy)methoxy)benzene
CAS No.:956024-18-3
Molecular Formula:C₆₆H₅₈O₁₂
Molecular Weight:1043.18
Hs Code.:

Synonyms:3,6-di(p-(phenylacetoxy)phenyl)-1,2,4,5-tetrakis((benzyloxy)methoxy)benzene

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Chemical Property of 3,6-di(p-(phenylacetoxy)phenyl)-1,2,4,5-tetrakis((benzyloxy)methoxy)benzene

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Technology Process of 3,6-di(p-(phenylacetoxy)phenyl)-1,2,4,5-tetrakis((benzyloxy)methoxy)benzene

There total 4 articles about 3,6-di(p-(phenylacetoxy)phenyl)-1,2,4,5-tetrakis((benzyloxy)methoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 956024-17-2
3,6-di(p-hydroxyphenyl)-1,2,4,5-tetrakis((benzyloxy)methoxy)benzene

: 103-80-0
phenylacetyl chloride

: 956024-18-3
3,6-di(p-(phenylacetoxy)phenyl)-1,2,4,5-tetrakis((benzyloxy)methoxy)benzene

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; at 20 ℃; for 0.5h;
DOI:10.1021/ol701590b

Reference yield:

: 102964-38-5
C₆H₄Br₂O₄

: 956024-18-3
3,6-di(p-(phenylacetoxy)phenyl)-1,2,4,5-tetrakis((benzyloxy)methoxy)benzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide / 0.5 h / 0 °C

1.2: 2.50 g / dimethylformamide / 14 h / 0 - 14 °C

2.1: 83 percent / Na₂CO₃; Ph₃P / Pd(OAc)2 / propan-1-ol; H₂O / 11 h / 100 °C

3.1: 79 percent / n-BuLi / tetrahydrofuran; hexane / 0.5 h / 20 °C

With n-butyllithium; sodium hydride; sodium carbonate; triphenylphosphine; palladium diacetate; In tetrahydrofuran; propan-1-ol; hexane; water; N,N-dimethyl-formamide; 2.1: Suzuki coupling;
DOI:10.1021/ol701590b

Reference yield:

: 956024-16-1
1,2,4,5-tetrakis((benzyloxy)methoxy)-3,5-dibromobenzene

: 956024-18-3
3,6-di(p-(phenylacetoxy)phenyl)-1,2,4,5-tetrakis((benzyloxy)methoxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / Na₂CO₃; Ph₃P / Pd(OAc)2 / propan-1-ol; H₂O / 11 h / 100 °C

2: 79 percent / n-BuLi / tetrahydrofuran; hexane / 0.5 h / 20 °C

With n-butyllithium; sodium carbonate; triphenylphosphine; palladium diacetate; In tetrahydrofuran; propan-1-ol; hexane; water; 1: Suzuki coupling;
DOI:10.1021/ol701590b