1-(4-Methoxy-phenyl)-3-oxo-1,3-dihydro-2-oxa-4,6-diaza-cyclopenta[c]fluorene-6-sulfonic acid dimethylamide

Base Information

Chemical Name:1-(4-Methoxy-phenyl)-3-oxo-1,3-dihydro-2-oxa-4,6-diaza-cyclopenta[c]fluorene-6-sulfonic acid dimethylamide
CAS No.:200809-37-6
Molecular Formula:C₂₂H₁₉N₃O₅S
Molecular Weight:437.476
Hs Code.:

Synonyms:1-(4-Methoxy-phenyl)-3-oxo-1,3-dihydro-2-oxa-4,6-diaza-cyclopenta[c]fluorene-6-sulfonic acid dimethylamide

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Chemical Property of 1-(4-Methoxy-phenyl)-3-oxo-1,3-dihydro-2-oxa-4,6-diaza-cyclopenta[c]fluorene-6-sulfonic acid dimethylamide

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Technology Process of 1-(4-Methoxy-phenyl)-3-oxo-1,3-dihydro-2-oxa-4,6-diaza-cyclopenta[c]fluorene-6-sulfonic acid dimethylamide

There total 3 articles about 1-(4-Methoxy-phenyl)-3-oxo-1,3-dihydro-2-oxa-4,6-diaza-cyclopenta[c]fluorene-6-sulfonic acid dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74214-62-3
ethyl 9H-pyrido[3,4-b]indole-3-carboxylate

: 200809-37-6
1-(4-Methoxy-phenyl)-3-oxo-1,3-dihydro-2-oxa-4,6-diaza-cyclopenta[c]fluorene-6-sulfonic acid dimethylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) trimethylaluminum / 1.) CH₂Cl₂, hexane, 2.) CH₂Cl₂, hexane, reflux

2: 93 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

3: 1.) MeLi, 2.) conc. H₂SO₄ / 1.) THF, -78 deg C, 30 min, then room temp., 2 h, 2.) CH₃CN, 30 min, room temp.

With sulfuric acid; methyllithium; trimethylaluminum; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo971485l

Reference yield:

: 78538-86-0
3-N-phenyl-β-carboline-3-carboxamide

: 200809-37-6
1-(4-Methoxy-phenyl)-3-oxo-1,3-dihydro-2-oxa-4,6-diaza-cyclopenta[c]fluorene-6-sulfonic acid dimethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / NaH / tetrahydrofuran / 3 h / Ambient temperature

2: 1.) MeLi, 2.) conc. H₂SO₄ / 1.) THF, -78 deg C, 30 min, then room temp., 2 h, 2.) CH₃CN, 30 min, room temp.

With sulfuric acid; methyllithium; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jo971485l

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 200809-36-5
9-(N,N-dimethylsulfamoyl)-β-carboline-3-(N-phenyl)carboxamide

: 200809-37-6
1-(4-Methoxy-phenyl)-3-oxo-1,3-dihydro-2-oxa-4,6-diaza-cyclopenta[c]fluorene-6-sulfonic acid dimethylamide

Guidance literature:: With sulfuric acid; methyllithium; Yield given. Multistep reaction; 1.) THF, -78 deg C, 30 min, then room temp., 2 h, 2.) CH₃CN, 30 min, room temp.;
DOI:10.1021/jo971485l