1-bromo-3-(4-ethylbenzyl)-5-(1-methoxy-D-glucopyranos-1-yl)-2-methyl-benzene

Base Information

Chemical Name:1-bromo-3-(4-ethylbenzyl)-5-(1-methoxy-D-glucopyranos-1-yl)-2-methyl-benzene
CAS No.:1050200-97-9
Molecular Formula:C₂₃H₂₉BrO₆
Molecular Weight:481.384
Hs Code.:

Synonyms:1-bromo-3-(4-ethylbenzyl)-5-(1-methoxy-D-glucopyranos-1-yl)-2-methyl-benzene

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Chemical Property of 1-bromo-3-(4-ethylbenzyl)-5-(1-methoxy-D-glucopyranos-1-yl)-2-methyl-benzene

Chemical Property:

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Technology Process of 1-bromo-3-(4-ethylbenzyl)-5-(1-methoxy-D-glucopyranos-1-yl)-2-methyl-benzene

There total 6 articles about 1-bromo-3-(4-ethylbenzyl)-5-(1-methoxy-D-glucopyranos-1-yl)-2-methyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1022983-62-5
3-bromo-5-(4-ethyl-benzyl)-1-iodo-4-methyl-benzene

: 32469-28-6,55515-28-1,55515-29-2,32384-65-9
(3R,4S,5R,6R)-3,4,5-tris((trimethylsilyl)oxy)-6-(((trimethylsilyl)oxy)methyl)tetrahydro-2H-pyran-2-one

: 1050200-97-9
1-bromo-3-(4-ethylbenzyl)-5-(1-methoxy-D-glucopyranos-1-yl)-2-methyl-benzene

Guidance literature:: 3-bromo-5-(4-ethyl-benzyl)-1-iodo-4-methyl-benzene; With TurboGrignard; In tetrahydrofuran; at -60 - -20 ℃; for 1h;

(3R,4S,5R,6R)-3,4,5-tris((trimethylsilyl)oxy)-6-(((trimethylsilyl)oxy)methyl)tetrahydro-2H-pyran-2-one; In tetrahydrofuran; at -20 - -5 ℃; for 6h;

methanol; With methanesulfonic acid; at 40 ℃; for 6h;

Reference yield:

: 76006-33-2
3-bromo-2-methylbenzoic acid

: 1050200-97-9
1-bromo-3-(4-ethylbenzyl)-5-(1-methoxy-D-glucopyranos-1-yl)-2-methyl-benzene

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-iodo-succinimide; sulfuric acid / 5 - 20 °C

2.1: thionyl chloride / N,N-dimethyl-formamide / 1 h / Heating / reflux

3.1: aluminum (III) chloride / dichloromethane / 2 h / 0 - 20 °C

4.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / 14.05 h / 0 - 20 °C

5.1: TurboGrignard / tetrahydrofuran / 1 h / -60 - -20 °C

5.2: 6 h / -20 - -5 °C

5.3: 6 h / 40 °C

With triethylsilane; aluminum (III) chloride; N-iodo-succinimide; TurboGrignard; thionyl chloride; sulfuric acid; boron trifluoride diethyl etherate; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; acetonitrile;

Reference yield:

: 1022983-50-1
3-bromo-5-iodo-2-methyl-benzoic acid

: 1050200-97-9
1-bromo-3-(4-ethylbenzyl)-5-(1-methoxy-D-glucopyranos-1-yl)-2-methyl-benzene

Guidance literature:: Multi-step reaction with 4 steps

1.1: thionyl chloride / N,N-dimethyl-formamide / 1 h / Heating / reflux

2.1: aluminum (III) chloride / dichloromethane / 2 h / 0 - 20 °C

3.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane; acetonitrile / 14.05 h / 0 - 20 °C

4.1: TurboGrignard / tetrahydrofuran / 1 h / -60 - -20 °C

4.2: 6 h / -20 - -5 °C

4.3: 6 h / 40 °C

With triethylsilane; aluminum (III) chloride; TurboGrignard; thionyl chloride; boron trifluoride diethyl etherate; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; acetonitrile;