(CH₃CH₂)4N⁽¹⁺⁾*W((C₆H₅)CCO)((C₄H₃N)CHNCH₃)2(CO)^(1-) = [(CH₃CH₂)4N][W((C₆H₅)CCO)((C₄H₃N)CHNCH₃)2(CO)]

Base Information

• Chemical Name: (CH₃CH₂)4N⁽¹⁺⁾*W((C₆H₅)CCO)((C₄H₃N)CHNCH₃)2(CO)^(1-) = [(CH₃CH₂)4N][W((C₆H₅)CCO)((C₄H₃N)CHNCH₃)2(CO)]
• CAS No.: 108452-78-4
• Molecular Formula: C₈H₂₀N*C₂₁H₁₉N₄O₂W
• Molecular Weight: 673.511

Synonyms:(CH₃CH₂)4N⁽¹⁺⁾*W((C₆H₅)CCO)((C₄H₃N)CHNCH₃)2(CO)^(1-) = [(CH₃CH₂)4N][W((C₆H₅)CCO)((C₄H₃N)CHNCH₃)2(CO)]

Chemical Property of (CH₃CH₂)4N⁽¹⁺⁾*W((C₆H₅)CCO)((C₄H₃N)CHNCH₃)2(CO)^(1-) = [(CH₃CH₂)4N][W((C₆H₅)CCO)((C₄H₃N)CHNCH₃)2(CO)]

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Technology Process of (CH₃CH₂)4N⁽¹⁺⁾*W((C₆H₅)CCO)((C₄H₃N)CHNCH₃)2(CO)^(1-) = [(CH₃CH₂)4N][W((C₆H₅)CCO)((C₄H₃N)CHNCH₃)2(CO)]

There total 1 articles about (CH₃CH₂)4N⁽¹⁺⁾*W((C₆H₅)CCO)((C₄H₃N)CHNCH₃)2(CO)^(1-) = [(CH₃CH₂)4N][W((C₆H₅)CCO)((C₄H₃N)CHNCH₃)2(CO)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-<(methylimino)methyl>pyrrole (15191-65-8) + W(CC6H5)Cl(CO)2(C5H5N)2 (99630-91-8) + tetraethylammonium chloride (56-34-8) → (CH3CH2)4N(1+)*W((C6H5)CCO)((C4H3N)CHNCH3)2(CO)(1-) = [(CH3CH2)4N][W((C6H5)CCO)((C4H3N)CHNCH3)2(CO)] (108452-78-4)

Guidance literature:

With KOH; In tetrahydrofuran; byproducts: KCl; (inert atmosphere); KOH pellets added to soln. of W compd. and the imine; 1.25 h stirred; react. mechanism discussed; solvent removed; washing (pentane); suspn. in CH2Cl2; (NEt4)Cl added; the solid dissolved and KClpptd.; stirring for 30 min; filtration (cellulose); filtrate concd.; ether dropwise added until an oily ppt. started to form; upon trituration of the ppt. and further addn. of ether crystals formed; elem. anal.; mass spectrum (mol. peak); Kinetics;

DOI:10.1021/om00150a023

Reference yield: 58.0%

Methyl fluorosulfonate (421-20-5) + (CH3CH2)4N(1+)*W((C6H5)CCO)((C4H3N)CHNCH3)2(CO)(1-) = [(CH3CH2)4N][W((C6H5)CCO)((C4H3N)CHNCH3)2(CO)] (108452-78-4) → W((C6H5)C2OCH3)(CO)((C4H3N)CHNCH3)2 (108452-79-5)

Guidance literature:

In dichloromethane; (inert atmosphere); methyl fluorosulfate added to soln. of W compd. at -78 °C; soln. warmed to room temp.; solvent removed in vac.; chromy. through a 5-cm high layer of silica gel with CH2Cl2/pentane (2/1); recrystn. from CH2Cl2/pentane; single crystals obtained; elem. anal.; mass spectrum (mol. peak);

DOI:10.1021/om00150a023

upstream raw materials:

2-<(methylimino)methyl>pyrrole

W(CC₆H₅)Cl(CO)2(C₅H₅N)2

tetraethylammonium chloride

Downstream raw materials:

W((C₆H₅)C₂OCH₃)(CO)((C₄H₃N)CHNCH₃)2

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