C₁₇H₂₃NO₃

Base Information

• Chemical Name: C₁₇H₂₃NO₃
• CAS No.: 1233241-12-7
• Molecular Formula: C₁₇H₂₃NO₃
• Molecular Weight: 289.375
• Mol file: 1233241-12-7.mol

Synonyms:C₁₇H₂₃NO₃

Chemical Property of C₁₇H₂₃NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₇H₂₃NO₃

There total 2 articles about C₁₇H₂₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

methanol (67-56-1) + N-cyclohexyl-2-phenylpropenamide (7473-00-9) + carbon monoxide (201230-82-2) → C17H23NO3 (1233241-12-7)

Guidance literature:

With bis(triphenylphosphine)palladium(II) dichloride; water; at 110 ℃; for 6h; under 5171.62 Torr; regioselective reaction;

DOI:10.1016/j.tetlet.2010.04.053

Reference yield:

methanol (67-56-1) + N-cyclohexyl-2-phenylpropenamide (7473-00-9) + carbon monoxide (201230-82-2) → N-cyclohexyl-2-phenylpropanamide + C17H23NO3 (1233241-12-7)

Guidance literature:

With bis(triphenylphosphine)palladium(II) dichloride; In tetrahydrofuran; at 110 ℃; for 6h; under 5171.62 Torr;

DOI:10.1016/j.tetlet.2010.04.053

Reference yield: 61.0%

C17H23NO3 (1233241-12-7) → N-cyclohexyl-2-phenylsuccinimide (139477-41-1)

Guidance literature:

With calcium hydride; In N,N-dimethyl-formamide; at 50 ℃; for 12h;

DOI:10.1016/j.tetlet.2010.04.053

upstream raw materials:

methanol

N-cyclohexyl-2-phenylpropenamide

carbon monoxide

Downstream raw materials:

N-cyclohexyl-2-phenylsuccinimide

Refernces